微波辅助制备石墨烯量子点固定化纳米二氧化硅作为合成杂蒽的高效非均相纳米催化剂

IF 1.7 Q3 CHEMISTRY, ORGANIC
Somayeh Pahlavan Moghanlo, H. Valizadeh
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引用次数: 5

摘要

在微波辐照的绿色反应条件下制备了石墨烯量子点(GQDs)固定化纳米二氧化硅,并将其用作一种高效的非均相酸催化剂。通过FT-IR、PL、TEM、XRD、FE-SEM、EDS、TGA和ζ电位对纳米催化剂的结构进行了表征。使用新制备的催化剂以优异的产率合成了黄原衍生物,并且催化剂可以容易地回收和再循环5次,而不会显著损失其催化活性。通过FT-IR、H-NMR、C-NMR等波谱技术对产物的结构进行了确证。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Microwave-assisted preparation of graphene quantum dots immobilized nanosilica as an efficient heterogeneous nanocatalyst for the synthesis of xanthenes
Graphene quantum dots (GQDs) immobilized nanosilica was prepared under microwave irradiated green reaction conditions and was used as an efficient heterogeneous acid catalyst. The structure of nano-catalyst was characterized by FT-IR, PL, TEM, XRD, FE-SEM, EDS, TGA, and zeta potential. Xanthene derivatives were synthesized in excellent yields using the freshly prepared catalyst and the catalyst could be easily recovered and recycled for 5 times without significant loss of its catalytic activity. The structures of the resulted products were confirmed by FT-IR, H-NMR, C-NMR spectroscopic techniques.
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来源期刊
Organic Communications
Organic Communications CHEMISTRY, ORGANIC-
CiteScore
2.80
自引率
11.80%
发文量
21
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