N, N′-Dibutyloxamide

IF 0.6 Q4 CHEMISTRY, ORGANIC

Molbank Pub Date : 2023-06-29 DOI:10.3390/m1677

E. Podda, Eleanor Dodd, M. Arca, M. Aragoni, V. Lippolis, Simon J. Coles, Anna Pintus

引用次数: 0

摘要

N、用草酸二乙酯和正丁胺在乙醇中反应制备了N′-二丁基恶酰胺（1），并用微量分析技术、红外光谱和核磁共振波谱对其进行了表征。从1的乙腈溶液中获得适用于单晶X射线衍射（SC-XRD）的晶体，并且结构表征显示存在分子间氢键相互作用。

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N,N′-Dibutyloxamide

N,N′-dibutyloxamide (1) was prepared by reacting diethyloxalate with n-butylamine in ethyl alcohol and characterized by microanalytical techniques, FT-IR, and NMR spectroscopy. Crystals suitable for single crystal X-ray diffraction (SC-XRD) were obtained from an acetonitrile solution of 1, and the structural characterization showed the presence of intermolecular hydrogen bonding interactions.

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来源期刊

Molbank Chemistry-Physical and Theoretical Chemistry

CiteScore

0.70

自引率

33.30%

发文量

174

审稿时长

11 weeks

期刊介绍： •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)