自旋镀膜生长银薄膜纳米结构的还原效果

Ari A. Yatem
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引用次数: 0

摘要

银(Ag)薄膜纳米结构是通过一种可靠的称为自旋镀膜的方法在玻璃表面制备的。利用硝酸银(agno3)作为前驱体,在h2气氛中进行热还原,并进行一些化学还原,如硼氢化钠(nabh4)溶液和水合肼(n2h4)溶液。讨论了几种还原剂的作用。利用x射线衍射(XRD)、扫描电子显微镜(SEM)以及紫外-可见-近红外吸收光谱等技术对沉积银薄膜的结构、形貌和吸光度进行了表征和测量,以进一步研究还原过程如何影响银纳米颗粒的形成。因此,在h2气氛中的热还原比在硼氢化钠和水合肼溶液中的化学还原更有效,以生长一致尺寸的分散纳米银。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effect of reduction through the Spin Coating growing Silver thin Films Nanostructure
Silver (Ag) thin-film nanostructures are prepared on the glass surface through a dependable method called spin coating. Silver nitrate (AgNO 3 ) has been utilized as precursors, proceeded by the thermal reduction in the H 2 atmosphere, and some of the chemical reductions such as sodium borohydride (NaBH 4 ) solution, and hydrazine hydrate solution (N 2 H 4 ). The effects of several reductants have been discussed. The structure, morphology, and absorbance spectra of the deposited silver thin films have been characterized and measured by using the following techniques X-ray diffraction (XRD), Scanning electron microscope (SEM), as well as UV-visible- NIR absorption spectroscopy, to study more about how the reduction procedure affects the formation of silver nanoparticles. As a result, thermal reduction in the H 2 atmosphere is more effective than the chemical reduction in aqueous sodium borohydride and hydrazine hydrate solution for growing consistently sized dispersed silver nanoparticles.
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来源期刊
CiteScore
0.50
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23
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