U. Osman, Sharmili Silvarajoo, I. Bhat, M. Razali, Mohd Zul Helmi Rozaini, T. B. Ravoof
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引用次数: 0
摘要
该化合物(Z)-4-[4-氟苯基]硫代氨基脲在单斜空间群p21 / c中结晶，晶胞参数为a = 12.1056(8)Å， b = 5.5177(4)Å， c = 12.5617(8)Å， β = 90.063(2)°，V = 839.06(10)Å 3, Z = 4。对结构进行求解，对数据进行细化，得到R和wR指数分别为0.0946和0.1377。在晶体中，每个分子通过两个N-H···S分子间氢键连接到下一个分子。
Crystal Structure of (Z)-4-[4-Fluorophenyl]thiosemicarbazide4
The present compound, namely ( Z )-4-[4-fluorophenyl]thiosemicarbazide, crystallized in a monoclinic space group, P 2 1 / c , with cell parameters a = 12.1056(8)Å, b = 5.5177(4)Å, c = 12.5617(8)Å, β = 90.063(2) ° , V = 839.06(10)Å 3 , and Z = 4. The structure was solved and the data was refined to reach R and wR indices of 0.0946 and 0.1377, respectively. In the crystal, each molecule was linked to the next molecule by two N–H···S intermolecular hydrogen bonds.
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