腈在碱性介质中选择性部分水解合成酰胺

化学与化工:英文版 Pub Date : 2020-06-28 DOI:10.17265/1934-7375/2020.02.003

Raymundo Yáñez-Alarid, Elvira Santos-Santos, Eva F. Lejarazo-Gómez

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引用次数: 1

摘要

采用传统的溶剂回流加热和超声波两种不同的能量源，将腈部分水解得到酰胺。用两种能量源分别在微、半微尺度和不同反应时间下进行了反应。用气相色谱法测定微尺度下的收率和半微尺度下的失重。

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Amide Synthesis through Selective Partial Hydrolysis of Nitriles in Alkaline Media

Amides were obtained through partial hydrolysis of nitriles, using two different energy sources, traditional heating with solvent reflux and ultrasound. The reaction was performed at micro and semi-micro scales and at different reaction time with both energy sources. Yield was determined through gas chromatography, in the case of micro-scale and weight loss in the case of semi-micro scale.

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化学与化工:英文版

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