以morpholine硼烷为还原剂化学沉积镍硼涂层

IF 0.5 4区 化学 Q4 CHEMISTRY, MULTIDISCIPLINARY
Chemija Pub Date : 2020-02-26 DOI:10.6001/chemija.v31i1.4167
Z. Sukackienė, K. Antanavičiūtė, J. Vaičiūnienė, L. Tamašauskaitė-Tamašiūnaitė, A. Naujokaitis, E. Norkus
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引用次数: 5

摘要

物理科学与技术中心催化系,立陶宛维尔纽斯索尔特基奥大道3号,10257。使用镍甘氨酸(Ni-Gly)电镀溶液和吗啉硼烷(MB)作为还原剂,在铜上沉积镍硼(NiB)涂层。已经确定,在Ni-Gly电镀溶液中使用MB作为还原剂可以产生NiB涂层,其表现出典型的花椰菜状纹理。NiB涂层的沉积速率及其组成取决于还原剂(MB)和配体(Gly)的浓度以及电镀溶液的pH和温度。当镀浴在pH 5和60°C温度下操作时,获得了NiB涂层的最高沉积速率(3.42 mg cm–2 h–1)。使用这种方法,可以获得含有10-20at.%硼的NiB涂层。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Electroless deposition of nickel boron coatings using morpholine borane as a reducing agent
Department of Catalysis, Center for Physical Sciences and Technology, 3 Saulėtekio Avenue, 10257 Vilnius, Lithuania Nickel boron (NiB) coatings were deposited onto copper using a nickelglycine (Ni-Gly) plating solution and morpholine borane (MB) as a reducing agent. It has been determined that using MB as a reducing agent in the Ni-Gly plating solution produces NiB coatings, which exhibit typical cauliflower-like textures. The deposition rate of the NiB coatings and their composition depend on the concentrations of the reducing agent (MB) and the ligand (Gly), in addition to the pH and temperature of the plating solution. The highest deposition rate (3.42 mg cm–2 h–1) of the NiB coating was obtained when the plating bath was operated at pH 5 and 60°C temperature. Using this method, NiB coatings containing 10–20 at.% of boron can be obtained.
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来源期刊
Chemija
Chemija 化学-化学综合
CiteScore
1.30
自引率
16.70%
发文量
14
审稿时长
>12 weeks
期刊介绍: Chemija publishes original research articles and reviews from all branches of modern chemistry, including physical, inorganic, analytical, organic, polymer chemistry, electrochemistry, and multidisciplinary approaches.
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