{"title":"水基滤饼改性提高井筒第二界面黏结强度的实验研究","authors":"Kevin Nsolloh Lichinga","doi":"10.1016/j.ptlrs.2022.10.002","DOIUrl":null,"url":null,"abstract":"<div><p>The objective of this experimental study is to improve the cementing bond quality of sandstone oil-gas well along the wellbore cement-formation interface (WCFI), so as to ensure long-term zonal isolation throughout the lifecycle of the well by using NSO solution as filtercake modifier which was developed in the laboratory. According to designed experimental method and API RP 10, the effectiveness of filtercake modifier (NSO) on the bonding strength at the WCFI was assessed by using designed simulated wellbore as sandstone formation. The experimental results indicated that the samples which were treated with NSO solution had higher bond strength over untreated samples. The strength generally increased with curing period as for treated samples, 0.198, 0.374, 0.433 and 0.473 MPa for 3, 7, 15, and 30 days respectively while for the untreated samples the bond strength were 0.050, 0.070, 0.81 and 0.100 MPa for the same period. The water-based filtercake modification techniques had significantly enhanced the bonding strength of WCFI by increasing rates above 296%. Improvement of bond strength to the treated sample was due to filtercake modification as a result of formation of cementitious material as revealed in FTIR spectral such as Calcium-Silicate-Hydrate (C–S–H) and other geopolymers like Calcium-Aluminium-Silicate-Hydrate (C-A-S-H) and Sodium-Aluminium-Silicate-Hydrate (N-A-S-H)) along the interface which filled the existed pores hence reducing porosity hence high strength of bond. The low transmittance value for the NSO treated samples revealed that there were more cementitious materials existing at the WCFI which led to improvement of bonding strength as compared to the untreated samples. The lower/poor bond strength for the untreated samples is due to existence of untreated, thick water-based filtercake films at WCFI, which prevented the complete hydration process between rock grains and cement slurry components to make chemical binder of cement slurry material and formation.</p></div>","PeriodicalId":19756,"journal":{"name":"Petroleum Research","volume":"8 4","pages":"Pages 531-540"},"PeriodicalIF":0.0000,"publicationDate":"2023-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S2096249522000667/pdfft?md5=581f8ebaa157869b2590e11c90172853&pid=1-s2.0-S2096249522000667-main.pdf","citationCount":"0","resultStr":"{\"title\":\"Experimental study on modification of water-based filtercake to improve the bonding strength at the wellbore cement-formation interface\",\"authors\":\"Kevin Nsolloh Lichinga\",\"doi\":\"10.1016/j.ptlrs.2022.10.002\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>The objective of this experimental study is to improve the cementing bond quality of sandstone oil-gas well along the wellbore cement-formation interface (WCFI), so as to ensure long-term zonal isolation throughout the lifecycle of the well by using NSO solution as filtercake modifier which was developed in the laboratory. According to designed experimental method and API RP 10, the effectiveness of filtercake modifier (NSO) on the bonding strength at the WCFI was assessed by using designed simulated wellbore as sandstone formation. The experimental results indicated that the samples which were treated with NSO solution had higher bond strength over untreated samples. The strength generally increased with curing period as for treated samples, 0.198, 0.374, 0.433 and 0.473 MPa for 3, 7, 15, and 30 days respectively while for the untreated samples the bond strength were 0.050, 0.070, 0.81 and 0.100 MPa for the same period. The water-based filtercake modification techniques had significantly enhanced the bonding strength of WCFI by increasing rates above 296%. Improvement of bond strength to the treated sample was due to filtercake modification as a result of formation of cementitious material as revealed in FTIR spectral such as Calcium-Silicate-Hydrate (C–S–H) and other geopolymers like Calcium-Aluminium-Silicate-Hydrate (C-A-S-H) and Sodium-Aluminium-Silicate-Hydrate (N-A-S-H)) along the interface which filled the existed pores hence reducing porosity hence high strength of bond. The low transmittance value for the NSO treated samples revealed that there were more cementitious materials existing at the WCFI which led to improvement of bonding strength as compared to the untreated samples. The lower/poor bond strength for the untreated samples is due to existence of untreated, thick water-based filtercake films at WCFI, which prevented the complete hydration process between rock grains and cement slurry components to make chemical binder of cement slurry material and formation.</p></div>\",\"PeriodicalId\":19756,\"journal\":{\"name\":\"Petroleum Research\",\"volume\":\"8 4\",\"pages\":\"Pages 531-540\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-12-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.sciencedirect.com/science/article/pii/S2096249522000667/pdfft?md5=581f8ebaa157869b2590e11c90172853&pid=1-s2.0-S2096249522000667-main.pdf\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Petroleum Research\",\"FirstCategoryId\":\"1087\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2096249522000667\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"Earth and Planetary Sciences\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Petroleum Research","FirstCategoryId":"1087","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2096249522000667","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"Earth and Planetary Sciences","Score":null,"Total":0}
引用次数: 0
摘要
本实验研究的目的是通过实验室研制的NSO溶液作为滤饼改进剂,改善砂岩油气井沿井眼水泥-地层界面(WCFI)的固井质量,从而保证井全生命周期内的长期层间隔离。根据设计的实验方法和API RP 10,采用设计的砂岩地层模拟井眼,评价了滤饼改性剂(NSO)对WCFI黏结强度的影响。实验结果表明,用NSO溶液处理的样品比未处理的样品具有更高的粘结强度。随着龄期的延长,粘结强度普遍增大,处理后3、7、15、30 d的粘结强度分别为0.198、0.374、0.433、0.473 MPa,而未处理后3、7、15、30 d的粘结强度分别为0.050、0.070、0.81、0.100 MPa。水基滤饼改性技术显著提高了WCFI的结合强度,提高率达到296%以上。处理后样品的结合强度的提高是由于滤饼的改性导致沿界面形成胶凝物质,如水合硅酸钙(C-S-H)和其他地聚合物,如水合硅酸钙-铝(C-A-S-H)和水合硅酸钠-铝(N-A-S-H),这些地聚合物填充了存在的孔隙,从而降低了孔隙率,从而提高了结合强度。NSO处理样品的低透光率值表明,与未处理样品相比,WCFI处存在更多的胶凝物质,从而导致粘接强度提高。未处理样品的粘结强度较低或较差是由于未处理的、较厚的水基滤饼膜在WCFI处存在,阻碍了岩石颗粒与水泥浆组分之间的完全水化过程,无法形成水泥浆材料和地层的化学粘结剂。
Experimental study on modification of water-based filtercake to improve the bonding strength at the wellbore cement-formation interface
The objective of this experimental study is to improve the cementing bond quality of sandstone oil-gas well along the wellbore cement-formation interface (WCFI), so as to ensure long-term zonal isolation throughout the lifecycle of the well by using NSO solution as filtercake modifier which was developed in the laboratory. According to designed experimental method and API RP 10, the effectiveness of filtercake modifier (NSO) on the bonding strength at the WCFI was assessed by using designed simulated wellbore as sandstone formation. The experimental results indicated that the samples which were treated with NSO solution had higher bond strength over untreated samples. The strength generally increased with curing period as for treated samples, 0.198, 0.374, 0.433 and 0.473 MPa for 3, 7, 15, and 30 days respectively while for the untreated samples the bond strength were 0.050, 0.070, 0.81 and 0.100 MPa for the same period. The water-based filtercake modification techniques had significantly enhanced the bonding strength of WCFI by increasing rates above 296%. Improvement of bond strength to the treated sample was due to filtercake modification as a result of formation of cementitious material as revealed in FTIR spectral such as Calcium-Silicate-Hydrate (C–S–H) and other geopolymers like Calcium-Aluminium-Silicate-Hydrate (C-A-S-H) and Sodium-Aluminium-Silicate-Hydrate (N-A-S-H)) along the interface which filled the existed pores hence reducing porosity hence high strength of bond. The low transmittance value for the NSO treated samples revealed that there were more cementitious materials existing at the WCFI which led to improvement of bonding strength as compared to the untreated samples. The lower/poor bond strength for the untreated samples is due to existence of untreated, thick water-based filtercake films at WCFI, which prevented the complete hydration process between rock grains and cement slurry components to make chemical binder of cement slurry material and formation.