“Pondoh Super”蛇果仁中羧甲基纤维素(CMC)的合成与表征

S. Anggrahini, D. Marsono, A. Setiyoko, A. Wahyuningtyas
{"title":"“Pondoh Super”蛇果仁中羧甲基纤维素(CMC)的合成与表征","authors":"S. Anggrahini, D. Marsono, A. Setiyoko, A. Wahyuningtyas","doi":"10.22146/IFNP.29778","DOIUrl":null,"url":null,"abstract":"Snake fruits kernel has high cellulose content thus potential to be an alternative source of carboxylmethylcellulose (CMC) production. However there are several condition that have to be optimized to increase the CMC synthesis which are concentration of  NaOH solution, NaMCA addition, and the reaction temperature based on  the degree of substitution (DS). The aim of this study was to determine the optimum conditions of synthesis CMC from “Salak Pondoh Super” kernel. Some factors that likely influence the synthesis were concentration of  NaOH solution , NaMCA addition, and the reaction temperature based on  the degree of substitution (DS) as the responses. Synthesis of CMC was optimized using completely randomized design. The result then was characterized by several parameters including water content, viscosity, purity, Water Holding Capacity (WHC), Oil Holding Capacity (OHC), lightness, crystallinity, and FT-IR spectra. Optimization was achieved by the use of  15% NaOH solution, 5 gram NaMCA per 5 gram cellulose and reaction temperature of 55oC. The characteristics of the optimized CMC were DS 0.825, purity 90.86%, water content of 7.16 (% wb), viscosity 3.86 cps, 142.72 yield (% db), WHC 2.37 (g/g), OHC 2.31 (g/g), lightness 78.48, and crystanillity 32.69%. The FT-IR spectra of snake fruit kernel CMC was similar with the CMC Standard.","PeriodicalId":13468,"journal":{"name":"Indonesian Food and Nutrition Progress","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2017-11-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":"{\"title\":\"Carboxymethyl Celulose (CMC) from Snake Fruit (Salaca edulis Reinw) Kernel of “Pondoh Super”: Synthesis and Characterization\",\"authors\":\"S. Anggrahini, D. Marsono, A. Setiyoko, A. Wahyuningtyas\",\"doi\":\"10.22146/IFNP.29778\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Snake fruits kernel has high cellulose content thus potential to be an alternative source of carboxylmethylcellulose (CMC) production. However there are several condition that have to be optimized to increase the CMC synthesis which are concentration of  NaOH solution, NaMCA addition, and the reaction temperature based on  the degree of substitution (DS). The aim of this study was to determine the optimum conditions of synthesis CMC from “Salak Pondoh Super” kernel. Some factors that likely influence the synthesis were concentration of  NaOH solution , NaMCA addition, and the reaction temperature based on  the degree of substitution (DS) as the responses. Synthesis of CMC was optimized using completely randomized design. The result then was characterized by several parameters including water content, viscosity, purity, Water Holding Capacity (WHC), Oil Holding Capacity (OHC), lightness, crystallinity, and FT-IR spectra. Optimization was achieved by the use of  15% NaOH solution, 5 gram NaMCA per 5 gram cellulose and reaction temperature of 55oC. The characteristics of the optimized CMC were DS 0.825, purity 90.86%, water content of 7.16 (% wb), viscosity 3.86 cps, 142.72 yield (% db), WHC 2.37 (g/g), OHC 2.31 (g/g), lightness 78.48, and crystanillity 32.69%. The FT-IR spectra of snake fruit kernel CMC was similar with the CMC Standard.\",\"PeriodicalId\":13468,\"journal\":{\"name\":\"Indonesian Food and Nutrition Progress\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2017-11-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Indonesian Food and Nutrition Progress\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.22146/IFNP.29778\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Indonesian Food and Nutrition Progress","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.22146/IFNP.29778","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 5

摘要

蛇果仁纤维素含量高,因此有潜力成为羧甲基纤维素(CMC)生产的替代来源。但要提高CMC的合成效率,还需要优化NaOH溶液的浓度、NaMCA的加入量和基于取代度的反应温度。本研究的目的是确定以超级沙叻蓬都仁为原料合成CMC的最佳工艺条件。影响合成的因素主要有NaOH溶液浓度、NaMCA加入量和基于取代度(DS)的反应温度。采用完全随机设计优化CMC的合成。然后用含水量、粘度、纯度、持水量(WHC)、持油量(OHC)、亮度、结晶度和FT-IR光谱等参数对结果进行表征。优化条件为NaOH浓度为15%,NaMCA浓度为5 g / 5 g,反应温度为55℃。优化后的CMC性能为:DS 0.825,纯度90.86%,含水量7.16 (% wb),粘度3.86 cps,收率142.72 (% db), WHC 2.37 (g/g), OHC 2.31 (g/g),亮度78.48,结晶度32.69%。蛇果仁CMC的FT-IR光谱与CMC标准相似。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Carboxymethyl Celulose (CMC) from Snake Fruit (Salaca edulis Reinw) Kernel of “Pondoh Super”: Synthesis and Characterization
Snake fruits kernel has high cellulose content thus potential to be an alternative source of carboxylmethylcellulose (CMC) production. However there are several condition that have to be optimized to increase the CMC synthesis which are concentration of  NaOH solution, NaMCA addition, and the reaction temperature based on  the degree of substitution (DS). The aim of this study was to determine the optimum conditions of synthesis CMC from “Salak Pondoh Super” kernel. Some factors that likely influence the synthesis were concentration of  NaOH solution , NaMCA addition, and the reaction temperature based on  the degree of substitution (DS) as the responses. Synthesis of CMC was optimized using completely randomized design. The result then was characterized by several parameters including water content, viscosity, purity, Water Holding Capacity (WHC), Oil Holding Capacity (OHC), lightness, crystallinity, and FT-IR spectra. Optimization was achieved by the use of  15% NaOH solution, 5 gram NaMCA per 5 gram cellulose and reaction temperature of 55oC. The characteristics of the optimized CMC were DS 0.825, purity 90.86%, water content of 7.16 (% wb), viscosity 3.86 cps, 142.72 yield (% db), WHC 2.37 (g/g), OHC 2.31 (g/g), lightness 78.48, and crystanillity 32.69%. The FT-IR spectra of snake fruit kernel CMC was similar with the CMC Standard.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
8
审稿时长
8 weeks
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信