静电纺丝法制备壳聚糖-聚氧聚乙烯-木薯粉纳米纤维

Riesca Ayu Kusuma Wardhani, L. Asri, M. Nasir, B. S. Purwasasmita
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引用次数: 6

摘要

以壳聚糖、聚氧聚乙烯(PEO)和土芋粉(CE)为原料,采用静电纺丝法制备了纳米纤维。制备了壳聚糖- peo和壳聚糖- peo - ce粉两种不同的纳米纤维。较高的PEO浓度(3%壳聚糖-6%PEO) (w/v)使壳聚糖-PEO静电纺纳米纤维更均匀,无珠。将胶体CE粉加入到含有3%壳聚糖-6% peo的溶液中,CE粉的浓度分别为5%、15%和25% (w/v),制备了壳聚糖- peo -CE粉。扫描电镜结果表明,壳聚糖- peo纳米纤维的平均直径为128±41 nm,壳聚糖- peo - ce面粉纳米纤维的平均直径为159±45 nm。随着CE粉含量的增加,纳米纤维的直径增大。傅里叶变换红外光谱显示壳聚糖、PEO和CE粉的特征峰存在。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Preparation of Chitosan-Polyethylene Oxide-Colocasia esculenta Flour Nanofibers using Electrospinning Method
Nanofibers have been prepared from the mixture of chitosan, polyethylene oxide (PEO) and Colocasia esculenta flour (CE flour) by using the electrospinning method. Two different nanofibers were formulated, containing chitosan-PEO and chitosan-PEO-CE flour. The higher concentration of PEO (3%chitosan-6%PEO) (w/v) resulted in more uniform chitosan-PEO electrospun nanofibers without beads. Chitosan-PEO-CE flour was prepared by addition of colloidal CE flour into the solution containing 3%chitosan-6%PEO with variation of the CE flour concentration of 5, 15 and 25% (w/v). Scanning Electron Microscopy demonstrated that the average diameter of chitosan-PEO nanofibers was 128±41 nm, whereas the diameter of chitosan-PEO-CE flour nanofibers was 159±45 nm. The diameters of nanofibers increased with the increase of CE flour content. Fourier transform infrared spectra demonstrate the presence characteristic peaks of chitosan, PEO and CE flour.
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