[CO(SALEN)(PPH3)(H2O)]4[Fe

A. Kianfar, N. Eskandari, M. A. Arayesh
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引用次数: 0

摘要

本文报道了[Co(Salen)(PPh3)(H2O)]4[Fe(CN)6]和[Co(Salophen)(PPh3)(H2O)]4[Fe(CN)6]希夫碱配合物的合成。将这些配合物在500、550和600℃下煅烧制备了Co3O4/CoFe2O4磁性纳米颗粒。用红外光谱和紫外-可见光谱对前驱物进行了鉴定,并用热重分析/差热分析研究了前驱物的热行为。采用x射线衍射(XRD)、扫描电镜(یکینورتکلا تسپ ،تابتاکم لوئسم:: akianfar@cc.iut.ac.ir)等方法对纳米磁性样品进行了表征,并对样品进行了纳米磁性表征
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis, Characterization and Investigation of Magnetic Properties of Co3O4/CoFe2O4 Nanocomposite Prepared by Calcination of [CO(SALEN)(PPH3)(H2O)]4[Fe(CN)6] and [Co(Salophen)(PPH3)(H2O)]4[Fe(CN)6] Binary Complex Salts
In this research the synthesis of [Co(Salen)(PPh3)(H2O)]4[Fe(CN)6] and [Co(Salophen)(PPh3)(H2O)]4[Fe(CN)6] schiff base complexes was reported. Co3O4/CoFe2O4 magnetic nanoparticles were prepared by calcination of these complexes at 500, 550 and 600°C. Precursor complexes were identified by FT-IR and UV-Vis spectroscopy and their thermal behavior was studied via TG/DTA. Nanomagnetic samples were characterized by X-ray diffraction (XRD), Scanning Electron Microscopy * یکینورتکلا تسپ ،تابتاکم لوئسم : : akianfar@cc.iut.ac.ir D ow nl oa de d fr om ja m e. iu t.a c. ir at 3 :4 4 IR S T o n S un da y N ov em be r 22 nd 2 02 0
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