慢蒸发法合成有机-无机杂化Fe3O（TFBDC）3（H2O）3·（DMF）3化合物：表征和磁性能比较

IF 0.3 4区物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY

Lithuanian Journal of Physics Pub Date : 2020-02-05 DOI:10.3952/physics.v60i1.4166

A. Laurikėnas, K. Mažeika, D. Baltrunas, R. Skaudžius, A. Beganskiene, A. Kareiva

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引用次数: 2

摘要

在合成有机-无机杂化Fe3O（TFBDC）3（H2O）3·（DMF）3化合物的研究中，提出了一种缓慢蒸发的方法。使用X射线粉末衍射（XRD）分析、扫描电子显微镜（SEM）和能量色散X射线光谱（EDX）结合SEM和电子顺磁共振（EPR）光谱对合成产物进行了表征。通过磁化测量和穆斯堡尔谱证实了合成样品的反铁磁/弱铁磁行为。合成的磁性材料本身可以测试用于不同的医学应用，并且可以用作制备具有多种生物医学有用性能的纳米结构氧化铁的前体材料。

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Hybrid organic-inorganic Fe3O(TFBDC)3(H2O)3·(DMF)3 compound synthesized by slow evaporation method: Characterization and comparison of magnetic properties

In this study for the synthesis of a hybrid organic-inorganic Fe3O(TFBDC)3(H2O)3·(DMF)3 compound a slow evaporation method has been suggested. THe synthesis product was characterized using X-ray powder diffraction (XRD) analysis, scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX) coupled with SEM and electron paramagnetic resonance (EPR) spectroscopy. THe antiferromagnetic/weakly ferromagnetic behaviour of the synthesized sample was confirmed by magnetization measurements and Mössbauer spectroscopy. THe synthesized magnetic material could be itself tested for different medical applications and could be used as precursor material for the preparation of nanostructured iron oxides with a variety of useful properties for biomedicine.

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来源期刊

Lithuanian Journal of Physics 物理-物理：综合

CiteScore

0.90

自引率

16.70%

发文量

审稿时长

>12 weeks

期刊介绍： The main aim of the Lithuanian Journal of Physics is to reflect the most recent advances in various fields of theoretical, experimental, and applied physics, including: mathematical and computational physics; subatomic physics; atoms and molecules; chemical physics; electrodynamics and wave processes; nonlinear and coherent optics; spectroscopy.