{"title":"镍催化环戊烯芳基硼化反应。","authors":"Stephen R Sardini, M Kevin Brown","doi":"10.15227/orgsyn.097.0355","DOIUrl":null,"url":null,"abstract":"A 500-mL, three-necked, round-bottom flask (24/40 ground glass joint, Flask A) is equipped with a 4.5 x 1.75-cm magnetic stir bar (Teflon-coated, egg-shaped), a rubber septum, a glass stopper, and a vacuum adapter with a stopcock (in the open position; connected to a dual manifold with bubbler). Flask A is evacuated (0.3 mmHg), flame-dried, and allowed to cool to room temperature under vacuum (Figure 1). The flask is then backfilled with a nitrogen atmosphere.","PeriodicalId":520734,"journal":{"name":"Organic syntheses; an annual publication of satisfactory methods for the preparation of organic chemicals","volume":" ","pages":"355-367"},"PeriodicalIF":0.0000,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7824973/pdf/nihms-1660217.pdf","citationCount":"5","resultStr":"{\"title\":\"Nickel-Catalyzed Arylboration of Cyclopentene.\",\"authors\":\"Stephen R Sardini, M Kevin Brown\",\"doi\":\"10.15227/orgsyn.097.0355\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A 500-mL, three-necked, round-bottom flask (24/40 ground glass joint, Flask A) is equipped with a 4.5 x 1.75-cm magnetic stir bar (Teflon-coated, egg-shaped), a rubber septum, a glass stopper, and a vacuum adapter with a stopcock (in the open position; connected to a dual manifold with bubbler). Flask A is evacuated (0.3 mmHg), flame-dried, and allowed to cool to room temperature under vacuum (Figure 1). The flask is then backfilled with a nitrogen atmosphere.\",\"PeriodicalId\":520734,\"journal\":{\"name\":\"Organic syntheses; an annual publication of satisfactory methods for the preparation of organic chemicals\",\"volume\":\" \",\"pages\":\"355-367\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2020-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7824973/pdf/nihms-1660217.pdf\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Organic syntheses; an annual publication of satisfactory methods for the preparation of organic chemicals\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.15227/orgsyn.097.0355\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Organic syntheses; an annual publication of satisfactory methods for the preparation of organic chemicals","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.15227/orgsyn.097.0355","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
A 500-mL, three-necked, round-bottom flask (24/40 ground glass joint, Flask A) is equipped with a 4.5 x 1.75-cm magnetic stir bar (Teflon-coated, egg-shaped), a rubber septum, a glass stopper, and a vacuum adapter with a stopcock (in the open position; connected to a dual manifold with bubbler). Flask A is evacuated (0.3 mmHg), flame-dried, and allowed to cool to room temperature under vacuum (Figure 1). The flask is then backfilled with a nitrogen atmosphere.
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