Mary Kombolias, Jan Obrzut, Dianne L Poster, Karl Montgomery, Michael T Postek, Yaw S Obeng
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引用次数: 0
摘要
目前造纸和纸浆行业的产品组成和质量测试方法主要基于手动原位湿台化学技术。例如,确定纸张成分的标准方法,TAPPI T 401“纸张和纸板的纤维分析”,依赖于受过专门训练的分析员的经验和视力来确定存在的单个植物物种,并量化纸张中每种组成纤维类型的量。因此,需要一种利用分析物固有属性的快速、无损分析技术。在本文中,我们展示了介电光谱(DS)作为一种潜在的计量学的应用,以区分非木浆和木浆纤维。这种原位、非接触和无损评估方法具有固有的取证能力,也适用于计量能力研究和实时统计过程控制(SPC)等质量保证技术。应用:本文提供的介电光谱结果可以无损地测定纸制品中木质素的含量,原则上与TAPPI标准测试方法T 401的性能规范相当,并且应该能够在纸张测试实验室环境中实时验证印刷基材的来源。
Dielectric spectroscopic studies of biological material evolution and application to paper.
Current product composition and quality test methods for the paper and pulp industry are mainly based on manual ex-situ wet-bench chemistry techniques. For example, the standard method for determining the furnish of paper, TAPPI T 401 "Fiber analysis of paper and paperboard," relies on the experience and visual acuity of a specially trained analyst to determine the individual plant species present and to quantify the amount of each constituent fiber type in a sheet of paper. Thus, there is a need for a fast, nondestructive analytical technique that leverages intrinsic attributes of the analytes. In this paper, we demonstrate an application of dielectric spectroscopy (DS) as a potential metrology to differentiate between nonwood pulp and wood pulp fibers. This in-situ, noncontact and nondestructive assessment method has inherent forensic capabilities and is also amiable to quality assurance techniques such as gauge capability studies and real-time statistical process control (SPC).
Application: The dielectric spectroscopy results presented in this paper can nondestructively determine the amount of lignin in paper products and are in principle comparable to the performance specifications of the TAPPI Standard Test Method T 401 and should enable the sources of printing substrates to be both authenticated and validated in real time in a paper testing laboratory environment.
期刊介绍:
An internationally recognized technical publication for over 60 years, TAPPI Journal (TJ) publishes the latest and most relevant research on the forest products and related industries. A stringent peer-review process and distinguished editorial board of academic and industry experts set TAPPI Journal apart as a reliable source for impactful basic and applied research and technical reviews.
Available at no charge to TAPPI members, each issue of TAPPI Journal features research in pulp, paper, packaging, tissue, nonwovens, converting, bioenergy, nanotechnology or other innovative cellulosic-based products and technologies. Publishing in TAPPI Journal delivers your research to a global audience of colleagues, peers and employers.