Rasha A Azzam, Galal H Elgemeie, Rasha E Elsayed, Peter G Jones
{"title":"N'-[2-(苯并[d]噻唑-2-基)乙酰基]-4-甲基苯磺酰肼的晶体结构。","authors":"Rasha A Azzam, Galal H Elgemeie, Rasha E Elsayed, Peter G Jones","doi":"10.1107/S2056989017008738","DOIUrl":null,"url":null,"abstract":"<p><p>In the title compound, C<sub>16</sub>H<sub>15</sub>N<sub>3</sub>O<sub>3</sub>S<sub>2</sub>, the hydrazide N atom bonded to the C=O group is planar, whereas that bonded to the SO<sub>2</sub> group is pyramidally coordinated. The inter-planar angle between the ring systems is 40.71 (3)°. Mol-ecules are connected into ribbons parallel to the <i>b</i> axis by two classical hydrogen bonds N-H⋯O=C and N-H⋯N<sub>thia-zole</sub>.</p>","PeriodicalId":7015,"journal":{"name":"Acta Crystallographica Section E Crystallographic Communications","volume":" ","pages":"1041-1043"},"PeriodicalIF":0.0000,"publicationDate":"2017-06-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5499286/pdf/","citationCount":"8","resultStr":"{\"title\":\"Crystal structure of <i>N</i>'-[2-(benzo[<i>d</i>]thia-zol-2-yl)acet-yl]-4-methyl-benzene-sulfono-hydrazide.\",\"authors\":\"Rasha A Azzam, Galal H Elgemeie, Rasha E Elsayed, Peter G Jones\",\"doi\":\"10.1107/S2056989017008738\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>In the title compound, C<sub>16</sub>H<sub>15</sub>N<sub>3</sub>O<sub>3</sub>S<sub>2</sub>, the hydrazide N atom bonded to the C=O group is planar, whereas that bonded to the SO<sub>2</sub> group is pyramidally coordinated. The inter-planar angle between the ring systems is 40.71 (3)°. Mol-ecules are connected into ribbons parallel to the <i>b</i> axis by two classical hydrogen bonds N-H⋯O=C and N-H⋯N<sub>thia-zole</sub>.</p>\",\"PeriodicalId\":7015,\"journal\":{\"name\":\"Acta Crystallographica Section E Crystallographic Communications\",\"volume\":\" \",\"pages\":\"1041-1043\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2017-06-16\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5499286/pdf/\",\"citationCount\":\"8\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta Crystallographica Section E Crystallographic Communications\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1107/S2056989017008738\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2017/7/1 0:00:00\",\"PubModel\":\"eCollection\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Crystallographica Section E Crystallographic Communications","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1107/S2056989017008738","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2017/7/1 0:00:00","PubModel":"eCollection","JCR":"","JCRName":"","Score":null,"Total":0}
Crystal structure of N'-[2-(benzo[d]thia-zol-2-yl)acet-yl]-4-methyl-benzene-sulfono-hydrazide.
In the title compound, C16H15N3O3S2, the hydrazide N atom bonded to the C=O group is planar, whereas that bonded to the SO2 group is pyramidally coordinated. The inter-planar angle between the ring systems is 40.71 (3)°. Mol-ecules are connected into ribbons parallel to the b axis by two classical hydrogen bonds N-H⋯O=C and N-H⋯Nthia-zole.
![Crystal structure of <i>N</i>'-[2-(benzo[<i>d</i>]thia-zol-2-yl)acet-yl]-4-methyl-benzene-sulfono-hydrazide.](https://img.booksci.cn/booksciimg/2017-6/2023121178217701643362243332870.jpg)
![Crystal structure of <i>N</i>'-[2-(benzo[<i>d</i>]thia-zol-2-yl)acet-yl]-4-methyl-benzene-sulfono-hydrazide.](https://img.booksci.cn/booksciimg/2017-6/2023121178256419178290068902569.jpg)
![Crystal structure of <i>N</i>'-[2-(benzo[<i>d</i>]thia-zol-2-yl)acet-yl]-4-methyl-benzene-sulfono-hydrazide.](https://img.booksci.cn/booksciimg/2017-6/2023121178296710089828737745736.jpg)
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