热液老化后整体氧化锆和堆芯氧化锆的半透明性。

Salma M Fathy, Abeer A El-Fallal, Salwa A El-Negoly, Abu Baker El Bedawy
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引用次数: 45

摘要

目的:评价水热老化对部分稳定的含氧化钇(Y-TZP)单晶氧化锆、全磨氧化锆和芯型氧化锆的透光性的影响。方法:将Y-TZP单片型和芯型材料各20个(1和10 mm)圆盘状试样,按照生产厂家的说明书进行铣削和烧结。根据使用的Y-TZP类型将最终标本分为两组。用漫反射法在白色和黑色背景上测量半透明参数(TP);采用x射线衍射(XRD)和扫描电子显微镜(SEM)对两种Y-TZP合金时效前后的微观结构进行了分析。TP值数据采用Student’st检验进行统计学分析。结果:整体Y-TZP老化前TP均值最高(16.4±0.316),而核心Y-TZP老化后TP均值最低(7.05±0.261)。热液老化前后两种Y-TZP类型存在显著差异。XRD分析表明,时效后两种Y-TZP表面的单斜晶含量均有所增加。结论:单片Y-TZP的低温降解率高于芯型,这可能会显著影响半透明Y-TZP的外观和透明度,从而影响其耐久性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Translucency of monolithic and core zirconia after hydrothermal aging.

Translucency of monolithic and core zirconia after hydrothermal aging.

Translucency of monolithic and core zirconia after hydrothermal aging.

Translucency of monolithic and core zirconia after hydrothermal aging.

Objective: To evaluate the hydrothermal aging effect on the translucency of partially stabilized tetragonal zirconia with yttria (Y-TZP) used as monolithic or fully milled zirconia and of core type. Methods: Twenty disc-shaped specimens (1 and 10 mm) for each type of monolithic and core Y-TZP materials were milled and sintered according to the manufacturer's instruction. The final specimens were divided into two groups according to the type of Y-TZP used. Translucency parameter (TP) was measured over white and black backgrounds with the diffuse reflectance method; X-ray diffraction (XRD) and scanning electron microscope (SEM) were used to analyze the microstructure of both Y-TZP types before and after aging. Data for TP values was statistically analyzed using Student's t-test. Results: Monolithic Y-TZP showed the highest TP mean value (16.4 ± 0.316) before aging while core Y-TZP showed the lowest TP mean value (7.05 ± 0.261) after aging. There was a significant difference between the two Y-TZP types before and after hydrothermal aging. XRD analysis showed increases in monoclinic content in both Y-TZP surfaces after aging. Conclusion: Monolithic Y-TZP has a higher chance to low-temperature degradation than core type, which may significantly affect the esthetic appearance and translucency hence durability of translucent Y-TZP.

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