1-苄基-4-(2,4-二氯苯基)-2-亚胺-1,2,5,6,7,8,9,10-八元-氢环八元-[b]吡啶-3-碳腈的晶体结构。

IF 0.9

Acta crystallographica. Section E, Structure reports online Pub Date : 2014-10-31 eCollection Date: 2014-11-01 DOI:10.1107/S1600536814023071

R A Nagalakshmi, J Suresh, S Maharani, R Ranjith Kumar, P L Nilantha Lakshman

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引用次数: 0

摘要

在标题化合物C25H23Cl2N3中，环辛烯环呈扭椅-椅构象。中心吡啶环(均方根偏差= 0.013 Å)与悬垂的氯苯环和苯基环的二面角分别为78.07(11)°和87.47(12)°。晶体中不存在方向性相互作用，排列受范德华相互作用支配。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

Crystal structure of 1-benzyl-4-(2,4-di-chloro-phenyl)-2-imino-1,2,5,6,7,8,9,10-octa-hydro-cyclo-octa-[b]pyridine-3-carbo-nitrile.

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Crystal structure of 1-benzyl-4-(2,4-di-chloro-phenyl)-2-imino-1,2,5,6,7,8,9,10-octa-hydro-cyclo-octa-[b]pyridine-3-carbo-nitrile.

In the title compound, C25H23Cl2N3, the cyclo-octene ring adopts a twist chair-chair conformation. The dihedral angles between the central pyridine ring (r.m.s. deviation = 0.013 Å) and the pendant chloro-benzene and benzyl rings are 78.07 (11) and 87.47 (12)°, respectively. No directional inter-actions could be identified in the crystal and the packing is governed by van der Waals inter-actions.

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来源期刊

Acta crystallographica. Section E, Structure reports online 化学-晶体学

自引率

33.30%

发文量

审稿时长

1.3 months

期刊介绍： Acta Crystallographica Section E: Structure Reports Online is the IUCr highly popular open-access structural journal. It provides a simple and easily accessible publication mechanism for the growing number of inorganic, metal-organic and organic crystal structure determinations. The electronic submission, validation, refereeing and publication facilities of the journal ensure very rapid and high-quality publication, whilst key indicators and validation reports provide measures of structural reliability. In 2009, the journal published over 4000 structures. The average publication time is less than one month.