Z.J. Xie , L.Q. Bai , X.F. Lu , X.L. Wang , R.D.K. Misra , C.J. Shang
{"title":"纳米析出物和位错对贝氏体钢轨钢强度和疲劳性能的协同作用","authors":"Z.J. Xie , L.Q. Bai , X.F. Lu , X.L. Wang , R.D.K. Misra , C.J. Shang","doi":"10.1016/j.ijfatigue.2025.109310","DOIUrl":null,"url":null,"abstract":"<div><div>This study examines the effect of tempering at 300–500 °C after forced-air cooling on fatigue properties of bainitic rail steel. Microstructural studies revealed that the specimens subjected to the four different heat treatments consisted of lath bainite and film-like retained austenite. The dislocation density for forced-air cooled, 300 °C, 400 °C, and 500 °C tempered conditions were 9.4 × 10<sup>14</sup> m<sup>−2</sup>, 7.9 × 10<sup>14</sup> m<sup>−2</sup>, 6.5 × 10<sup>14</sup> m<sup>−2</sup>, and 4.1 × 10<sup>14</sup> m<sup>−2</sup>, respectively. V(C,N) precipitates larger than 20 nm were primarily observed in the forced-air cooled steel, exhibited a unimodal size distribution with an average particle size of ∼ 25 nm. Tempering at 300 °C had minimal influence on the precipitation behavior. After tempering at 400 °C and 500 °C, new nano-size VC precipitates with an average particle size of 7.8 nm were observed, exhibiting a bimodal size distribution. At 400 °C, the strengthening effect of nano-size precipitates outweighs softening due to dislocation recovery, resulting in highest yield strength and fatigue limit. Fatigue fracture analysis revealed that the 500 °C tempered steel exhibited interior inclusion-induced crack initiation, while samples subjected to other heat treatments showed crack initiation from the surface or surface inclusions. Newly formed small grains were observed only at the crack initiation site induced by internal inclusions in the 500 °C tempered steel. This indicated that high-temperature tempering significantly reduced the dislocation density, which is detrimental to fatigue behavior. The optimal fatigue performance at 400 °C ascribed to the balanced synergy between moderate dislocation density and nano-precipitation. This finding provides new strategy to design bainitic rail steels with high fatigue property.</div></div>","PeriodicalId":14112,"journal":{"name":"International Journal of Fatigue","volume":"203 ","pages":"Article 109310"},"PeriodicalIF":6.8000,"publicationDate":"2025-09-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synergistic effect of nano-size precipitations and dislocations on the strength and fatigue behavior of bainitic rail steel\",\"authors\":\"Z.J. Xie , L.Q. Bai , X.F. Lu , X.L. Wang , R.D.K. Misra , C.J. Shang\",\"doi\":\"10.1016/j.ijfatigue.2025.109310\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>This study examines the effect of tempering at 300–500 °C after forced-air cooling on fatigue properties of bainitic rail steel. Microstructural studies revealed that the specimens subjected to the four different heat treatments consisted of lath bainite and film-like retained austenite. The dislocation density for forced-air cooled, 300 °C, 400 °C, and 500 °C tempered conditions were 9.4 × 10<sup>14</sup> m<sup>−2</sup>, 7.9 × 10<sup>14</sup> m<sup>−2</sup>, 6.5 × 10<sup>14</sup> m<sup>−2</sup>, and 4.1 × 10<sup>14</sup> m<sup>−2</sup>, respectively. V(C,N) precipitates larger than 20 nm were primarily observed in the forced-air cooled steel, exhibited a unimodal size distribution with an average particle size of ∼ 25 nm. Tempering at 300 °C had minimal influence on the precipitation behavior. After tempering at 400 °C and 500 °C, new nano-size VC precipitates with an average particle size of 7.8 nm were observed, exhibiting a bimodal size distribution. At 400 °C, the strengthening effect of nano-size precipitates outweighs softening due to dislocation recovery, resulting in highest yield strength and fatigue limit. Fatigue fracture analysis revealed that the 500 °C tempered steel exhibited interior inclusion-induced crack initiation, while samples subjected to other heat treatments showed crack initiation from the surface or surface inclusions. Newly formed small grains were observed only at the crack initiation site induced by internal inclusions in the 500 °C tempered steel. This indicated that high-temperature tempering significantly reduced the dislocation density, which is detrimental to fatigue behavior. The optimal fatigue performance at 400 °C ascribed to the balanced synergy between moderate dislocation density and nano-precipitation. This finding provides new strategy to design bainitic rail steels with high fatigue property.</div></div>\",\"PeriodicalId\":14112,\"journal\":{\"name\":\"International Journal of Fatigue\",\"volume\":\"203 \",\"pages\":\"Article 109310\"},\"PeriodicalIF\":6.8000,\"publicationDate\":\"2025-09-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Fatigue\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0142112325005079\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"ENGINEERING, MECHANICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Fatigue","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0142112325005079","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MECHANICAL","Score":null,"Total":0}
Synergistic effect of nano-size precipitations and dislocations on the strength and fatigue behavior of bainitic rail steel
This study examines the effect of tempering at 300–500 °C after forced-air cooling on fatigue properties of bainitic rail steel. Microstructural studies revealed that the specimens subjected to the four different heat treatments consisted of lath bainite and film-like retained austenite. The dislocation density for forced-air cooled, 300 °C, 400 °C, and 500 °C tempered conditions were 9.4 × 1014 m−2, 7.9 × 1014 m−2, 6.5 × 1014 m−2, and 4.1 × 1014 m−2, respectively. V(C,N) precipitates larger than 20 nm were primarily observed in the forced-air cooled steel, exhibited a unimodal size distribution with an average particle size of ∼ 25 nm. Tempering at 300 °C had minimal influence on the precipitation behavior. After tempering at 400 °C and 500 °C, new nano-size VC precipitates with an average particle size of 7.8 nm were observed, exhibiting a bimodal size distribution. At 400 °C, the strengthening effect of nano-size precipitates outweighs softening due to dislocation recovery, resulting in highest yield strength and fatigue limit. Fatigue fracture analysis revealed that the 500 °C tempered steel exhibited interior inclusion-induced crack initiation, while samples subjected to other heat treatments showed crack initiation from the surface or surface inclusions. Newly formed small grains were observed only at the crack initiation site induced by internal inclusions in the 500 °C tempered steel. This indicated that high-temperature tempering significantly reduced the dislocation density, which is detrimental to fatigue behavior. The optimal fatigue performance at 400 °C ascribed to the balanced synergy between moderate dislocation density and nano-precipitation. This finding provides new strategy to design bainitic rail steels with high fatigue property.
期刊介绍:
Typical subjects discussed in International Journal of Fatigue address:
Novel fatigue testing and characterization methods (new kinds of fatigue tests, critical evaluation of existing methods, in situ measurement of fatigue degradation, non-contact field measurements)
Multiaxial fatigue and complex loading effects of materials and structures, exploring state-of-the-art concepts in degradation under cyclic loading
Fatigue in the very high cycle regime, including failure mode transitions from surface to subsurface, effects of surface treatment, processing, and loading conditions
Modeling (including degradation processes and related driving forces, multiscale/multi-resolution methods, computational hierarchical and concurrent methods for coupled component and material responses, novel methods for notch root analysis, fracture mechanics, damage mechanics, crack growth kinetics, life prediction and durability, and prediction of stochastic fatigue behavior reflecting microstructure and service conditions)
Models for early stages of fatigue crack formation and growth that explicitly consider microstructure and relevant materials science aspects
Understanding the influence or manufacturing and processing route on fatigue degradation, and embedding this understanding in more predictive schemes for mitigation and design against fatigue
Prognosis and damage state awareness (including sensors, monitoring, methodology, interactive control, accelerated methods, data interpretation)
Applications of technologies associated with fatigue and their implications for structural integrity and reliability. This includes issues related to design, operation and maintenance, i.e., life cycle engineering
Smart materials and structures that can sense and mitigate fatigue degradation
Fatigue of devices and structures at small scales, including effects of process route and surfaces/interfaces.