Yi Ba , Jiaxing Guo , Miaoning Yan , Liang Guo , Qingmao Zhang
{"title":"选择性激光熔化NiTi合金织构演变及多机制强化研究","authors":"Yi Ba , Jiaxing Guo , Miaoning Yan , Liang Guo , Qingmao Zhang","doi":"10.1016/j.jmrt.2025.09.216","DOIUrl":null,"url":null,"abstract":"<div><div>The mechanical performance of NiTi alloys is strongly governed by microstructural features such as densification, grain morphology, and dislocation density. However, quantitative insights into how processing parameters systematically control grain size, high-angle grain boundary (HAGB) fraction, texture characteristics, and kernel average misorientation (KAM) to achieve targeted property tuning remain limited. This study integrates experimental analysis, thermo-fluid coupling simulations, and theoretical modeling to systematically investigate the effects of laser power (100–140 W) and scanning speed (900–1100 mm/s) on the densification behavior and microstructural evolution of NiTi alloys fabricated by selective laser melting (SLM). The simulations reveal the evolution of Marangoni convection within the melt pool under varying energy densities, while metallographic analysis quantifies the correlation between porosity and processing parameters. The optimal process parameters (130 W, 1000 mm/s) yielded a tensile strength of 549 MPa, elongation of 6.39 %, elastic modulus of 21.04 GPa, and microhardness of 316–321 HV. EBSD analysis showed HAGB fractions of 41.7 % (X–Z) and 41.4 % (X–Y), with average grain sizes of 19.03 μm and 27.44 μm. TEM revealed abundant linear dislocations and uniformly dispersed NiTi<sub>2</sub> precipitates. These results demonstrate that the combination of high densification, strong texture, and multiple strengthening mechanisms enables a favorable balance of strength and ductility, thereby providing both theoretical guidance and practical insights for optimizing SLM-processed NiTi alloys.</div></div>","PeriodicalId":54332,"journal":{"name":"Journal of Materials Research and Technology-Jmr&t","volume":"39 ","pages":"Pages 1960-1976"},"PeriodicalIF":6.6000,"publicationDate":"2025-09-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Investigation of texture evolution and multi-mechanism strengthening in NiTi alloy produced via selective laser melting\",\"authors\":\"Yi Ba , Jiaxing Guo , Miaoning Yan , Liang Guo , Qingmao Zhang\",\"doi\":\"10.1016/j.jmrt.2025.09.216\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The mechanical performance of NiTi alloys is strongly governed by microstructural features such as densification, grain morphology, and dislocation density. However, quantitative insights into how processing parameters systematically control grain size, high-angle grain boundary (HAGB) fraction, texture characteristics, and kernel average misorientation (KAM) to achieve targeted property tuning remain limited. This study integrates experimental analysis, thermo-fluid coupling simulations, and theoretical modeling to systematically investigate the effects of laser power (100–140 W) and scanning speed (900–1100 mm/s) on the densification behavior and microstructural evolution of NiTi alloys fabricated by selective laser melting (SLM). The simulations reveal the evolution of Marangoni convection within the melt pool under varying energy densities, while metallographic analysis quantifies the correlation between porosity and processing parameters. The optimal process parameters (130 W, 1000 mm/s) yielded a tensile strength of 549 MPa, elongation of 6.39 %, elastic modulus of 21.04 GPa, and microhardness of 316–321 HV. EBSD analysis showed HAGB fractions of 41.7 % (X–Z) and 41.4 % (X–Y), with average grain sizes of 19.03 μm and 27.44 μm. TEM revealed abundant linear dislocations and uniformly dispersed NiTi<sub>2</sub> precipitates. These results demonstrate that the combination of high densification, strong texture, and multiple strengthening mechanisms enables a favorable balance of strength and ductility, thereby providing both theoretical guidance and practical insights for optimizing SLM-processed NiTi alloys.</div></div>\",\"PeriodicalId\":54332,\"journal\":{\"name\":\"Journal of Materials Research and Technology-Jmr&t\",\"volume\":\"39 \",\"pages\":\"Pages 1960-1976\"},\"PeriodicalIF\":6.6000,\"publicationDate\":\"2025-09-23\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Materials Research and Technology-Jmr&t\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2238785425024706\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Materials Research and Technology-Jmr&t","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2238785425024706","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Investigation of texture evolution and multi-mechanism strengthening in NiTi alloy produced via selective laser melting
The mechanical performance of NiTi alloys is strongly governed by microstructural features such as densification, grain morphology, and dislocation density. However, quantitative insights into how processing parameters systematically control grain size, high-angle grain boundary (HAGB) fraction, texture characteristics, and kernel average misorientation (KAM) to achieve targeted property tuning remain limited. This study integrates experimental analysis, thermo-fluid coupling simulations, and theoretical modeling to systematically investigate the effects of laser power (100–140 W) and scanning speed (900–1100 mm/s) on the densification behavior and microstructural evolution of NiTi alloys fabricated by selective laser melting (SLM). The simulations reveal the evolution of Marangoni convection within the melt pool under varying energy densities, while metallographic analysis quantifies the correlation between porosity and processing parameters. The optimal process parameters (130 W, 1000 mm/s) yielded a tensile strength of 549 MPa, elongation of 6.39 %, elastic modulus of 21.04 GPa, and microhardness of 316–321 HV. EBSD analysis showed HAGB fractions of 41.7 % (X–Z) and 41.4 % (X–Y), with average grain sizes of 19.03 μm and 27.44 μm. TEM revealed abundant linear dislocations and uniformly dispersed NiTi2 precipitates. These results demonstrate that the combination of high densification, strong texture, and multiple strengthening mechanisms enables a favorable balance of strength and ductility, thereby providing both theoretical guidance and practical insights for optimizing SLM-processed NiTi alloys.
期刊介绍:
The Journal of Materials Research and Technology is a publication of ABM - Brazilian Metallurgical, Materials and Mining Association - and publishes four issues per year also with a free version online (www.jmrt.com.br). The journal provides an international medium for the publication of theoretical and experimental studies related to Metallurgy, Materials and Minerals research and technology. Appropriate submissions to the Journal of Materials Research and Technology should include scientific and/or engineering factors which affect processes and products in the Metallurgy, Materials and Mining areas.