V. T. Lebedev, V. S. Kozlov, M. V. Remizov, Yu. V. Kulvelis
{"title":"中子束在伽玛共振光谱中的应用前景","authors":"V. T. Lebedev, V. S. Kozlov, M. V. Remizov, Yu. V. Kulvelis","doi":"10.1007/s10512-025-01212-0","DOIUrl":null,"url":null,"abstract":"<div><p>A model of an electrodynamic Mössbauer spectrometer has been developed by the NRC “Kurchatov Institute”—PNPI (Gatchina, Russian Federation). The model represents a prototype using the neutron beam of the PIK reactor, which is generated using either constant or periodic activation of a γ-source, and isotope sources for structural and physicochemical studies of steel and alloys, minerals, catalysts, nanostructures, and biological objects. The article presents the physical characteristics of the model, as well as the sample preparation methodology and measurement modes with sample cooling to liquid nitrogen temperature. The experiments performed on a crystal hydrate with initially divalent iron admixed with Fe<sup>3+</sup> have demonstrated the capabilities of the spectrometer for non-destructive testing of chemical reactions. The potential of the spectrometer in nanotechnology is illustrated by the results of studying magnetic graphene oxide composites and nanodiamonds grafted with europium ions.</p></div>","PeriodicalId":480,"journal":{"name":"Atomic Energy","volume":"137 5-6","pages":"327 - 332"},"PeriodicalIF":0.3000,"publicationDate":"2025-06-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Prospects of using neutron beams for gamma-resonance spectroscopy\",\"authors\":\"V. T. Lebedev, V. S. Kozlov, M. V. Remizov, Yu. V. Kulvelis\",\"doi\":\"10.1007/s10512-025-01212-0\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>A model of an electrodynamic Mössbauer spectrometer has been developed by the NRC “Kurchatov Institute”—PNPI (Gatchina, Russian Federation). The model represents a prototype using the neutron beam of the PIK reactor, which is generated using either constant or periodic activation of a γ-source, and isotope sources for structural and physicochemical studies of steel and alloys, minerals, catalysts, nanostructures, and biological objects. The article presents the physical characteristics of the model, as well as the sample preparation methodology and measurement modes with sample cooling to liquid nitrogen temperature. The experiments performed on a crystal hydrate with initially divalent iron admixed with Fe<sup>3+</sup> have demonstrated the capabilities of the spectrometer for non-destructive testing of chemical reactions. The potential of the spectrometer in nanotechnology is illustrated by the results of studying magnetic graphene oxide composites and nanodiamonds grafted with europium ions.</p></div>\",\"PeriodicalId\":480,\"journal\":{\"name\":\"Atomic Energy\",\"volume\":\"137 5-6\",\"pages\":\"327 - 332\"},\"PeriodicalIF\":0.3000,\"publicationDate\":\"2025-06-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Atomic Energy\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s10512-025-01212-0\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"NUCLEAR SCIENCE & TECHNOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Atomic Energy","FirstCategoryId":"5","ListUrlMain":"https://link.springer.com/article/10.1007/s10512-025-01212-0","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"NUCLEAR SCIENCE & TECHNOLOGY","Score":null,"Total":0}
Prospects of using neutron beams for gamma-resonance spectroscopy
A model of an electrodynamic Mössbauer spectrometer has been developed by the NRC “Kurchatov Institute”—PNPI (Gatchina, Russian Federation). The model represents a prototype using the neutron beam of the PIK reactor, which is generated using either constant or periodic activation of a γ-source, and isotope sources for structural and physicochemical studies of steel and alloys, minerals, catalysts, nanostructures, and biological objects. The article presents the physical characteristics of the model, as well as the sample preparation methodology and measurement modes with sample cooling to liquid nitrogen temperature. The experiments performed on a crystal hydrate with initially divalent iron admixed with Fe3+ have demonstrated the capabilities of the spectrometer for non-destructive testing of chemical reactions. The potential of the spectrometer in nanotechnology is illustrated by the results of studying magnetic graphene oxide composites and nanodiamonds grafted with europium ions.
期刊介绍:
Atomic Energy publishes papers and review articles dealing with the latest developments in the peaceful uses of atomic energy. Topics include nuclear chemistry and physics, plasma physics, accelerator characteristics, reactor economics and engineering, applications of isotopes, and radiation monitoring and safety.