Yu. F. Kargin, Zh. V. Eremeeva, G. Kh. Sharipzyanova, D. A. Ushkalova
{"title":"机械合成锆酸镝粉坯的致密性和固结性","authors":"Yu. F. Kargin, Zh. V. Eremeeva, G. Kh. Sharipzyanova, D. A. Ushkalova","doi":"10.1134/S2075113325700996","DOIUrl":null,"url":null,"abstract":"<div><p>Dysprosium zirconate powder Dy<sub>2</sub>Zr<sub>2</sub>O<sub>7</sub> was obtained by mechanochemical synthesis of a stoichiometric mixture of zirconium oxide and dysprosium oxide. By X-ray phase analysis, as well as transmission and scanning electron microscopy, it has been demonstrated that the initial zirconium oxide and dysprosium oxide powders interact during mechanochemical synthesis for 30–45 min with the formation of the compound Dy<sub>2</sub>Zr<sub>2</sub>O<sub>7</sub>. The technological properties (fluidity, compactibility) of polycrystalline powders of mechanically synthesized dysprosium zirconate, as well as its microstructure after consolidation, have been studied.</p></div>","PeriodicalId":586,"journal":{"name":"Inorganic Materials: Applied Research","volume":"16 4","pages":"1038 - 1043"},"PeriodicalIF":0.3000,"publicationDate":"2025-08-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Features of Compactness and Consolidation of Blanks Made of Mechanically Synthesized Dysprosium Zirconate Powder\",\"authors\":\"Yu. F. Kargin, Zh. V. Eremeeva, G. Kh. Sharipzyanova, D. A. Ushkalova\",\"doi\":\"10.1134/S2075113325700996\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Dysprosium zirconate powder Dy<sub>2</sub>Zr<sub>2</sub>O<sub>7</sub> was obtained by mechanochemical synthesis of a stoichiometric mixture of zirconium oxide and dysprosium oxide. By X-ray phase analysis, as well as transmission and scanning electron microscopy, it has been demonstrated that the initial zirconium oxide and dysprosium oxide powders interact during mechanochemical synthesis for 30–45 min with the formation of the compound Dy<sub>2</sub>Zr<sub>2</sub>O<sub>7</sub>. The technological properties (fluidity, compactibility) of polycrystalline powders of mechanically synthesized dysprosium zirconate, as well as its microstructure after consolidation, have been studied.</p></div>\",\"PeriodicalId\":586,\"journal\":{\"name\":\"Inorganic Materials: Applied Research\",\"volume\":\"16 4\",\"pages\":\"1038 - 1043\"},\"PeriodicalIF\":0.3000,\"publicationDate\":\"2025-08-02\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Inorganic Materials: Applied Research\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S2075113325700996\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Inorganic Materials: Applied Research","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1134/S2075113325700996","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Features of Compactness and Consolidation of Blanks Made of Mechanically Synthesized Dysprosium Zirconate Powder
Dysprosium zirconate powder Dy2Zr2O7 was obtained by mechanochemical synthesis of a stoichiometric mixture of zirconium oxide and dysprosium oxide. By X-ray phase analysis, as well as transmission and scanning electron microscopy, it has been demonstrated that the initial zirconium oxide and dysprosium oxide powders interact during mechanochemical synthesis for 30–45 min with the formation of the compound Dy2Zr2O7. The technological properties (fluidity, compactibility) of polycrystalline powders of mechanically synthesized dysprosium zirconate, as well as its microstructure after consolidation, have been studied.
期刊介绍:
Inorganic Materials: Applied Research contains translations of research articles devoted to applied aspects of inorganic materials. Best articles are selected from four Russian periodicals: Materialovedenie, Perspektivnye Materialy, Fizika i Khimiya Obrabotki Materialov, and Voprosy Materialovedeniya and translated into English. The journal reports recent achievements in materials science: physical and chemical bases of materials science; effects of synergism in composite materials; computer simulations; creation of new materials (including carbon-based materials and ceramics, semiconductors, superconductors, composite materials, polymers, materials for nuclear engineering, materials for aircraft and space engineering, materials for quantum electronics, materials for electronics and optoelectronics, materials for nuclear and thermonuclear power engineering, radiation-hardened materials, materials for use in medicine, etc.); analytical techniques; structure–property relationships; nanostructures and nanotechnologies; advanced technologies; use of hydrogen in structural materials; and economic and environmental issues. The journal also considers engineering issues of materials processing with plasma, high-gradient crystallization, laser technology, and ultrasonic technology. Currently the journal does not accept direct submissions, but submissions to one of the source journals is possible.