Kai Sheng , Wenhao Liu , Ningrui Wang , Boliang Li , Longqing Chen , Bo Liu , Ding Ren , Jun Zhu , Ming Yin
{"title":"热等静压调节电子束粉末床熔合制备Ti-6Al-4V的组织和力学性能","authors":"Kai Sheng , Wenhao Liu , Ningrui Wang , Boliang Li , Longqing Chen , Bo Liu , Ding Ren , Jun Zhu , Ming Yin","doi":"10.1016/j.jmrt.2025.09.075","DOIUrl":null,"url":null,"abstract":"<div><div>Electron Beam Powder Bed Fusion Additive Manufacturing (EB-PBF AM) has gained significant industrial recognition due to its advantages in geometric design flexibility, functional integration, and integrated forming. However, EB-PBF fabricated parts are subject to internal gas pores and lack-of-fusion defects accompanied by the formation of metastable α′ martensite in microstructure. To address these challenges, this study employs hot isostatic pressing (HIP) post-processing for microstructure modification and defect elimination, systematically investigating the influence of HIP temperature (880 °C, 920 °C, 960 °C) on microstructure evolution and tensile properties of Ti–6Al–4V alloy. Experimental results demonstrate that the α phase undergoes significant coarsening with increasing HIP temperature, accompanied by the formation of spheroidized α phase particles. Variant selection analysis reveals a monotonic decrease in variant selection intensity with ascending HIP temperatures. After HIP treatment at 920 °C, the samples achieve optimal strength-ductility balance (ultimate tensile strength: 852 MPa, elongation: 18.2 %), primarily attributed to their moderate α phase dimensions and β phase content. Interestingly, despite α phase coarsening after 960 °C HIP compared to 920 °C HIP, the strength exhibits a paradoxical increase, which is attributed to a higher proportion of hard oriented α and the coarsening interface phase for the strengthening of interfacial barriers.</div></div>","PeriodicalId":54332,"journal":{"name":"Journal of Materials Research and Technology-Jmr&t","volume":"39 ","pages":"Pages 782-791"},"PeriodicalIF":6.6000,"publicationDate":"2025-09-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microstructure and mechanical properties of Ti–6Al–4V fabricated by electron beam powder bed fusion regulated via hot isostatic pressing\",\"authors\":\"Kai Sheng , Wenhao Liu , Ningrui Wang , Boliang Li , Longqing Chen , Bo Liu , Ding Ren , Jun Zhu , Ming Yin\",\"doi\":\"10.1016/j.jmrt.2025.09.075\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Electron Beam Powder Bed Fusion Additive Manufacturing (EB-PBF AM) has gained significant industrial recognition due to its advantages in geometric design flexibility, functional integration, and integrated forming. However, EB-PBF fabricated parts are subject to internal gas pores and lack-of-fusion defects accompanied by the formation of metastable α′ martensite in microstructure. To address these challenges, this study employs hot isostatic pressing (HIP) post-processing for microstructure modification and defect elimination, systematically investigating the influence of HIP temperature (880 °C, 920 °C, 960 °C) on microstructure evolution and tensile properties of Ti–6Al–4V alloy. Experimental results demonstrate that the α phase undergoes significant coarsening with increasing HIP temperature, accompanied by the formation of spheroidized α phase particles. Variant selection analysis reveals a monotonic decrease in variant selection intensity with ascending HIP temperatures. After HIP treatment at 920 °C, the samples achieve optimal strength-ductility balance (ultimate tensile strength: 852 MPa, elongation: 18.2 %), primarily attributed to their moderate α phase dimensions and β phase content. Interestingly, despite α phase coarsening after 960 °C HIP compared to 920 °C HIP, the strength exhibits a paradoxical increase, which is attributed to a higher proportion of hard oriented α and the coarsening interface phase for the strengthening of interfacial barriers.</div></div>\",\"PeriodicalId\":54332,\"journal\":{\"name\":\"Journal of Materials Research and Technology-Jmr&t\",\"volume\":\"39 \",\"pages\":\"Pages 782-791\"},\"PeriodicalIF\":6.6000,\"publicationDate\":\"2025-09-16\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Materials Research and Technology-Jmr&t\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2238785425023294\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Materials Research and Technology-Jmr&t","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2238785425023294","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Microstructure and mechanical properties of Ti–6Al–4V fabricated by electron beam powder bed fusion regulated via hot isostatic pressing
Electron Beam Powder Bed Fusion Additive Manufacturing (EB-PBF AM) has gained significant industrial recognition due to its advantages in geometric design flexibility, functional integration, and integrated forming. However, EB-PBF fabricated parts are subject to internal gas pores and lack-of-fusion defects accompanied by the formation of metastable α′ martensite in microstructure. To address these challenges, this study employs hot isostatic pressing (HIP) post-processing for microstructure modification and defect elimination, systematically investigating the influence of HIP temperature (880 °C, 920 °C, 960 °C) on microstructure evolution and tensile properties of Ti–6Al–4V alloy. Experimental results demonstrate that the α phase undergoes significant coarsening with increasing HIP temperature, accompanied by the formation of spheroidized α phase particles. Variant selection analysis reveals a monotonic decrease in variant selection intensity with ascending HIP temperatures. After HIP treatment at 920 °C, the samples achieve optimal strength-ductility balance (ultimate tensile strength: 852 MPa, elongation: 18.2 %), primarily attributed to their moderate α phase dimensions and β phase content. Interestingly, despite α phase coarsening after 960 °C HIP compared to 920 °C HIP, the strength exhibits a paradoxical increase, which is attributed to a higher proportion of hard oriented α and the coarsening interface phase for the strengthening of interfacial barriers.
期刊介绍:
The Journal of Materials Research and Technology is a publication of ABM - Brazilian Metallurgical, Materials and Mining Association - and publishes four issues per year also with a free version online (www.jmrt.com.br). The journal provides an international medium for the publication of theoretical and experimental studies related to Metallurgy, Materials and Minerals research and technology. Appropriate submissions to the Journal of Materials Research and Technology should include scientific and/or engineering factors which affect processes and products in the Metallurgy, Materials and Mining areas.