{"title":"4-苄基-4-戊基-morpholin-4-氯化铵的合成及晶体结构。","authors":"Zarifa Yakhshilikova , Tursunali Kholikov , Sherzod Zhurakulov , Kambarali Turgunov","doi":"10.1107/S2056989025006772","DOIUrl":null,"url":null,"abstract":"<div><div>An investigation is reported of the synthesis and crystal structure of 4-benzyl-4-pentylmorpholin-4-ium chloride</div></div><div><div>The reaction of <em>N</em>-pentylmorpholine with benzyl chloride resulted in the title compound, C<sub>16</sub>H<sub>26</sub>ClNO, which crystallizes in the orthorhombic space group <em>Pna</em>2<sub>1</sub> with <em>Z</em> = 4. In the crystal, the chloride ions are surrounded by four cations, forming layers.</div></div>","PeriodicalId":7367,"journal":{"name":"Acta Crystallographica Section E: Crystallographic Communications","volume":"81 9","pages":"Pages 797-800"},"PeriodicalIF":0.6000,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis and crystal structure of 4-benzyl-4-pentylmorpholin-4-ium chloride\",\"authors\":\"Zarifa Yakhshilikova , Tursunali Kholikov , Sherzod Zhurakulov , Kambarali Turgunov\",\"doi\":\"10.1107/S2056989025006772\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>An investigation is reported of the synthesis and crystal structure of 4-benzyl-4-pentylmorpholin-4-ium chloride</div></div><div><div>The reaction of <em>N</em>-pentylmorpholine with benzyl chloride resulted in the title compound, C<sub>16</sub>H<sub>26</sub>ClNO, which crystallizes in the orthorhombic space group <em>Pna</em>2<sub>1</sub> with <em>Z</em> = 4. In the crystal, the chloride ions are surrounded by four cations, forming layers.</div></div>\",\"PeriodicalId\":7367,\"journal\":{\"name\":\"Acta Crystallographica Section E: Crystallographic Communications\",\"volume\":\"81 9\",\"pages\":\"Pages 797-800\"},\"PeriodicalIF\":0.6000,\"publicationDate\":\"2025-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta Crystallographica Section E: Crystallographic Communications\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/org/science/article/pii/S2056989025001628\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CRYSTALLOGRAPHY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Crystallographica Section E: Crystallographic Communications","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/org/science/article/pii/S2056989025001628","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CRYSTALLOGRAPHY","Score":null,"Total":0}
引用次数: 0
摘要
n -戊基-啉与氯化苄反应生成标题化合物C16H26ClNO,该化合物在Z = 4的邻方阵空间群Pna21中结晶。在晶体中,氯离子被四个阳离子包围,形成层。
Synthesis and crystal structure of 4-benzyl-4-pentylmorpholin-4-ium chloride
An investigation is reported of the synthesis and crystal structure of 4-benzyl-4-pentylmorpholin-4-ium chloride
The reaction of N-pentylmorpholine with benzyl chloride resulted in the title compound, C16H26ClNO, which crystallizes in the orthorhombic space group Pna21 with Z = 4. In the crystal, the chloride ions are surrounded by four cations, forming layers.
期刊介绍:
Acta Crystallographica Section E: Crystallographic Communications is the IUCr''s open-access structural communications journal. It provides a fast, simple and easily accessible publication mechanism for crystal structure determinations of inorganic, metal-organic and organic compounds. The electronic submission, validation, refereeing and publication facilities of the journal ensure rapid and high-quality publication of fully validated structures. The primary article category is Research Communications; these are peer-reviewed articles describing one or more structure determinations with appropriate discussion of the science.