不同抛光工艺对slm打印牙科用Co-Cr合金表面形貌、耐蚀性和RPD框架适应性的影响。

IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE
Jiawen Gan, Hanzhi Zhang, Jian Sun, Chenyuan Zhu, Ting Jiao
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引用次数: 0

摘要

目的:比较电解抛光(EP)、等离子体电解抛光(PP)、干式电解抛光(DP)及其组合对选择性激光熔化(SLM)打印牙科用钴铬(Co-Cr)合金表面特性、耐腐蚀性和材料减量的影响。材料和方法:采用slm打印标准样品和可摘局部义齿(RPD)框架,然后采用以下方法抛光:机械抛光(MP), EP, PP, DP, PDP (PP + DP), DPP (DP + PP)和PDPP (PP + DP + PP)。利用光学轮廓术、扫描电子显微镜(SEM)和x射线光电子能谱(XPS)分析表面特征。通过电化学测试和离子释放实验对其耐蚀性进行了评价。通过测量重量损失、主要连接器和卡环厚度损失以及框架适应性来评估金属减量。记录技术人员对这些框架进行精细抛光的后处理时间,以进一步评估框架的抛光质量。所有测量结果均以均数±标准差表示。统计资料采用方差分析(ANOVA)和非参数单因素分析进行分析。结果:MP组的粗糙度最低(0.04±0.01µm),其次是PDPP组(0.49±0.12µm)。各组钝化膜成分均以Cr2O3为主,PDP组中有少量的cr3。PDPP表现出最小的离子释放(0.12µg/cm2)和稳定的Nyquist图。PDPP可以在不影响框架适应的情况下显著减少技术人员的后处理时间(45.75 s, p < 0.05)。结论:PDPP形成了稳定的钝化膜,离子释放极低,表面高度光滑均匀。这大大减少了人工后处理所需的时间,同时保持了RPD框架的准确性,使其非常适合大规模临床框架抛光。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effects of various polishing processes on surface morphology, corrosion resistance, and RPD framework adaptation of SLM-printed dental Co-Cr alloys.

Purpose: This in vitro study aims to compare the effects of electrolytic polishing (EP), plasma electrolytic polishing (PP), dry electropolishing (DP), and their combination on the surface characteristics, corrosion resistance, and material reduction of selective laser melting (SLM) printed dental cobalt-chromium (Co-Cr) alloy.

Materials and methods: Standard samples and removable partial denture (RPD) frameworks were SLM-printed and then polished using the following methods: mechanical polishing (MP), EP, PP, DP, PDP (PP + DP), DPP (DP + PP), and PDPP (PP + DP + PP). Surface characteristics were analyzed using optical profilometry, scanning electron microscopy (SEM), and x-ray photoelectron spectroscopy (XPS). Corrosion resistance was assessed through electrochemical testing and ion release experiments. The metal reduction was evaluated by measuring weight loss, major connector and clasp thickness loss, and framework adaptation. The post-processing time for the technician's fine polishing of these frameworks was recorded to further evaluate the polishing quality of the frameworks. All measurements were presented as mean ±standard deviation. Statistical data were analyzed using analysis of variance (ANOVA) and nonparametric one-way analysis.

Results: The MP group exhibited the lowest roughness (0.04 ± 0.01 µm), followed by the PDPP group (0.49 ± 0.12 µm). All groups had a passivation film composition predominantly composed of Cr2O3, with a small amount of CrO3 observed in the PDP group. PDPP exhibited minimal ion release (0.12 µg/cm2) and stable Nyquist plots. PDPP can significantly reduce the technician's post-processing time (45.75 s, p < 0.05) without compromising the adaptation of the frameworks.

Conclusions: PDPP forms a stable passivation film with extremely low ion release and a highly smooth, uniform surface. This significantly reduces the time required for manual post-processing while maintaining the accuracy of RPD frameworks, making it highly suitable for large-scale clinical framework polishing.

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来源期刊
CiteScore
7.90
自引率
15.00%
发文量
171
审稿时长
6-12 weeks
期刊介绍: The Journal of Prosthodontics promotes the advanced study and practice of prosthodontics, implant, esthetic, and reconstructive dentistry. It is the official journal of the American College of Prosthodontists, the American Dental Association-recognized voice of the Specialty of Prosthodontics. The journal publishes evidence-based original scientific articles presenting information that is relevant and useful to prosthodontists. Additionally, it publishes reports of innovative techniques, new instructional methodologies, and instructive clinical reports with an interdisciplinary flair. The journal is particularly focused on promoting the study and use of cutting-edge technology and positioning prosthodontists as the early-adopters of new technology in the dental community.
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