Shitan Ning , Xianglu Tang , Liang Xu , Wei Wu , Xuewen Shi , Zhenxue Jiang , Xinyue Zhang , Xinlei Wang
{"title":"基于像素信息的页岩无机组分孔隙定量识别方法","authors":"Shitan Ning , Xianglu Tang , Liang Xu , Wei Wu , Xuewen Shi , Zhenxue Jiang , Xinyue Zhang , Xinlei Wang","doi":"10.1016/j.ngib.2025.06.001","DOIUrl":null,"url":null,"abstract":"<div><div>The types and structures of inorganic pores are key factors in evaluations of the reservoir space and distribution characteristics of shale oil and gas. However, quantitative identification methods for pores of different inorganic components have not yet been fully developed. For this reason, a quantitative characterization method of inorganic pores using pixel information was proposed in this study. A machine learning algorithm was used to assist the field emission scanning electron microscopy (FE-SEM) image processing of shale to realize the accurate identification and quantitative characterization of inorganic pores on the surface of high-precision images of shale with a small view. Moreover, large-view image splicing technology, combined with quantitative evaluation of minerals by scanning electron microscopy (QEMSCAN) image joint characterization technology, was used to accurately analyze the distribution characteristics of inorganic pores under different mineral components. The quantitative methods of pore characteristics of different inorganic components under the pixel information of shale were studied. The results showed that (1) the Waikato Environment for Knowledge Analysis (WEKA) machine learning model can effectively identify and extract shale mineral components and inorganic pore distribution, and the large-view FE-SEM images are representative of samples at the 200 μm × 200 μm view scale, meeting statistical requirements and eliminating the influence of heterogeneity; (2) the pores developed by different mineral components of shale had obvious differences, indicating that the development of inorganic pores is highly correlated with the properties of shale minerals themselves; and (3) the pore-forming ability of different mineral components is calculated by the quantitative method of single component pore-forming coefficient. Chlorite showed the highest pore-forming ability, followed by (in descending order) illite, pyrite, calcite, dolomite, albite, orthoclase, quartz, and apatite. This study contributes to advancing our understanding of inorganic pore characteristics in shale.</div></div>","PeriodicalId":37116,"journal":{"name":"Natural Gas Industry B","volume":"12 4","pages":"Pages 447-461"},"PeriodicalIF":6.5000,"publicationDate":"2025-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Quantitative identification method for pores in shale inorganic components based on pixel information\",\"authors\":\"Shitan Ning , Xianglu Tang , Liang Xu , Wei Wu , Xuewen Shi , Zhenxue Jiang , Xinyue Zhang , Xinlei Wang\",\"doi\":\"10.1016/j.ngib.2025.06.001\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The types and structures of inorganic pores are key factors in evaluations of the reservoir space and distribution characteristics of shale oil and gas. However, quantitative identification methods for pores of different inorganic components have not yet been fully developed. For this reason, a quantitative characterization method of inorganic pores using pixel information was proposed in this study. A machine learning algorithm was used to assist the field emission scanning electron microscopy (FE-SEM) image processing of shale to realize the accurate identification and quantitative characterization of inorganic pores on the surface of high-precision images of shale with a small view. Moreover, large-view image splicing technology, combined with quantitative evaluation of minerals by scanning electron microscopy (QEMSCAN) image joint characterization technology, was used to accurately analyze the distribution characteristics of inorganic pores under different mineral components. The quantitative methods of pore characteristics of different inorganic components under the pixel information of shale were studied. The results showed that (1) the Waikato Environment for Knowledge Analysis (WEKA) machine learning model can effectively identify and extract shale mineral components and inorganic pore distribution, and the large-view FE-SEM images are representative of samples at the 200 μm × 200 μm view scale, meeting statistical requirements and eliminating the influence of heterogeneity; (2) the pores developed by different mineral components of shale had obvious differences, indicating that the development of inorganic pores is highly correlated with the properties of shale minerals themselves; and (3) the pore-forming ability of different mineral components is calculated by the quantitative method of single component pore-forming coefficient. Chlorite showed the highest pore-forming ability, followed by (in descending order) illite, pyrite, calcite, dolomite, albite, orthoclase, quartz, and apatite. This study contributes to advancing our understanding of inorganic pore characteristics in shale.</div></div>\",\"PeriodicalId\":37116,\"journal\":{\"name\":\"Natural Gas Industry B\",\"volume\":\"12 4\",\"pages\":\"Pages 447-461\"},\"PeriodicalIF\":6.5000,\"publicationDate\":\"2025-08-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Natural Gas Industry B\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2352854025000440\",\"RegionNum\":3,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"ENERGY & FUELS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Natural Gas Industry B","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2352854025000440","RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"ENERGY & FUELS","Score":null,"Total":0}
引用次数: 0
摘要
无机孔隙类型和结构是评价页岩油气储集空间和分布特征的关键因素。然而,不同无机组分孔隙的定量鉴定方法尚未完全成熟。为此,本研究提出了一种利用像元信息对无机孔隙进行定量表征的方法。利用机器学习算法辅助页岩场发射扫描电镜(FE-SEM)图像处理,实现了页岩小视野高精度图像表面无机孔隙的准确识别和定量表征。采用大视点图像拼接技术,结合扫描电镜(QEMSCAN)图像联合表征技术对矿物进行定量评价,准确分析不同矿物组分下无机孔隙的分布特征。研究了页岩像元信息下不同无机组分孔隙特征的定量方法。结果表明:(1)Waikato Environment for Knowledge Analysis (WEKA)机器学习模型能够有效识别和提取页岩矿物成分和无机孔隙分布,大视场FE-SEM图像在200 μm × 200 μm视场尺度下具有代表性,满足统计要求,消除了非均质性的影响;(2)页岩中不同矿物组分发育的孔隙存在明显差异,表明无机孔隙的发育与页岩矿物本身的性质高度相关;(3)采用单组分成孔系数定量方法计算不同矿物组分的成孔能力。绿泥石成孔能力最强,依次为伊利石、黄铁矿、方解石、白云石、钠长石、正长石、石英、磷灰石。该研究有助于加深对页岩无机孔隙特征的认识。
Quantitative identification method for pores in shale inorganic components based on pixel information
The types and structures of inorganic pores are key factors in evaluations of the reservoir space and distribution characteristics of shale oil and gas. However, quantitative identification methods for pores of different inorganic components have not yet been fully developed. For this reason, a quantitative characterization method of inorganic pores using pixel information was proposed in this study. A machine learning algorithm was used to assist the field emission scanning electron microscopy (FE-SEM) image processing of shale to realize the accurate identification and quantitative characterization of inorganic pores on the surface of high-precision images of shale with a small view. Moreover, large-view image splicing technology, combined with quantitative evaluation of minerals by scanning electron microscopy (QEMSCAN) image joint characterization technology, was used to accurately analyze the distribution characteristics of inorganic pores under different mineral components. The quantitative methods of pore characteristics of different inorganic components under the pixel information of shale were studied. The results showed that (1) the Waikato Environment for Knowledge Analysis (WEKA) machine learning model can effectively identify and extract shale mineral components and inorganic pore distribution, and the large-view FE-SEM images are representative of samples at the 200 μm × 200 μm view scale, meeting statistical requirements and eliminating the influence of heterogeneity; (2) the pores developed by different mineral components of shale had obvious differences, indicating that the development of inorganic pores is highly correlated with the properties of shale minerals themselves; and (3) the pore-forming ability of different mineral components is calculated by the quantitative method of single component pore-forming coefficient. Chlorite showed the highest pore-forming ability, followed by (in descending order) illite, pyrite, calcite, dolomite, albite, orthoclase, quartz, and apatite. This study contributes to advancing our understanding of inorganic pore characteristics in shale.