基于三维参数空间的EBSD标引方法提高了晶界标引性能

IF 2 3区 工程技术 Q2 MICROSCOPY
Fan Peng , Xuemei Song , Yiling Huang , Xingyu Jin , Yuqing Jiang , Yue Sun , Yi Zeng
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引用次数: 0

摘要

电子背散射衍射(EBSD)是基于扫描电子显微镜(SEM)的一项重要技术,它提供了广泛的晶体学信息。现有的模式标引方法有限,且大多为商业仪器制造商所掌握,这可能会制约标引技术的共享和发展。本文提出了一种基于三维参数空间的EBSD模式索引方法。该方法将特征三角形的表征扩展到三维参数空间。本文详细介绍了新索引算法的实现过程。利用从立方氧化钇稳定氧化锆(YSZ)散装样品中捕获的实验图案证明了这种新方法的实用性。与商业标引结果相比,该方法一致性好,在晶界处标引性能更好。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A new EBSD indexing method with enhanced grain boundary indexing performance using a three-dimensional parameter space
Electron backscatter diffraction (EBSD) is an important technique based on the scanning electron microscope (SEM) that provides a wide range of crystallographic information. There are limited available pattern indexing methods and most of them are mastered by commercial instrument manufacturers, which may probably restrict the sharing and development of indexing techniques. In this study, we present a new EBSD pattern indexing method based on a three-dimensional parameter space. This method extends the characterization of characteristic triangles into a three-dimensional parameter space. This work details the procedure of the new indexing algorithm. The utility of this new method is demonstrated using experimental patterns captured from a cubic yttria-stabilized zirconia (YSZ) bulk sample. Compared with commercial indexing results, the new method shows excellent consistency and achieves better indexing performance at grain boundaries.
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来源期刊
Ultramicroscopy
Ultramicroscopy 工程技术-显微镜技术
CiteScore
4.60
自引率
13.60%
发文量
117
审稿时长
5.3 months
期刊介绍: Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.
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