通过连续交替差速挤压,实现Mg-Gd-Y-Zn-Zr合金致密细晶组织的强度-塑性协同

IF 7.5 2区 材料科学 Q1 ENGINEERING, INDUSTRIAL
Dawei Meng , Yan Xu , Jianbo Jia , Bo Xu , Lianxi Hu
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引用次数: 0

摘要

挤压镁合金一直以来都存在严重的各向异性,这严重阻碍了其轻量化的广泛应用。为了克服这一持续的挑战,本研究提出了一种创新的连续交替差速挤压(CADSE)工艺,该工艺利用不对称应变场同时实现各向异性控制和力学性能增强。作为一个突破性的证明,Mg-Gd-Y-Zn-Zr合金板材同时提高了力学性能和降低了各向异性首次成功地采用CADSE工艺。系统研究了非对称空腔结构对铸坯组织演变、织构特征及变形机理的影响。此外,还阐明了挤压薄板保持细晶组织和增强强度-塑性的内在机制。结果表明,挤压后板材的力学性能得到了显著增强,其中E460(460°C挤压)板材的拉伸成形性能优于E430(430°C挤压)板材。E460-45°试样的抗拉屈服强度(TYS)为256 MPa,极限抗拉强度(UTS)为323 MPa,伸长率为22.7 %。强度的提高主要源于组织的细化、高硬度形变晶粒的保留以及再结晶晶粒内部层错的析出。相反,这种特殊的延性增强源于高比例的再结晶和消除晶间二次相。连续动态再结晶(CDRX)机制是整个CADSE过程的主要成核机制。相反,孪生诱导的动态再结晶(TDRX)机制在前两个通道中只起了很小的作用。此外,随着累积应变的增大,变形颗粒的主要变形方式由基底<;a>; 滑移转变为棱柱形<;a>; 滑移。再结晶晶界处溶质原子的偏析、再结晶晶内SFs的析出以及长周期有序堆积相(LPSO)的破碎化共同作用,有效抑制了挤压板材的显微组织粗化。CADSE工艺代表了金属成形技术的突破,为各向异性控制和力学性能增强建立了新的范式。这种创新的方法建立了适用于不同材料系统的挤压板制造的一般框架。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Achieving strength-ductility synergy of Mg-Gd-Y-Zn-Zr alloy with dense fine-grained microstructure via continuous alternating differential speed extrusion
Extruded magnesium (Mg) alloys have long been plagued by severe anisotropy, which severely impedes their widespread industrial application despite outstanding lightweight potential. To overcome this persistent challenge, an innovative continuous alternating differential speed extrusion (CADSE) process was proposed in this study, which utilizes asymmetric strain fields to concurrently achieve anisotropy control and mechanical performance enhancement. As a groundbreaking demonstration, Mg-Gd-Y-Zn-Zr alloy sheets with simultaneously enhanced mechanical performance and reduced anisotropy were successfully fabricated for the first time by employing the CADSE process. The effects of the asymmetric cavity structure on microstructure evolution, texture characteristics, and deformation mechanisms of the billet was systematically investigated during the CADSE process. Moreover, the intrinsic mechanisms for the retention of fine-grained structure and strength-ductility enhancement in the extruded sheets were also elucidated. The results indicated that the mechanical properties of the extruded sheets were significantly strengthened, with the E460 (extruded at 460 °C) sheet demonstrating superior stretch forming performance compared to the E430 (extruded at 430 °C) sheet. The superior combination of strength and ductility was obtained in the E460–45° sample, exhibiting tensile yield strength (TYS) of 256 MPa, ultimate tensile strength (UTS) of 323 MPa, and elongation of 22.7 %. The strength improvement originated from microstructural refinement, the retained high-hardness deformed grains, and the precipitation of stacking faults (SFs) within the recrystallized grains. In contrast, the exceptional ductility enhancement stemmed from high proportion of recrystallization and the elimination of intergranular secondary phases. The continuous dynamic recrystallization (CDRX) mechanism served as the primary nucleation mechanism throughout the CADSE process. Conversely, the twinning-induced dynamic recrystallization (TDRX) mechanism played merely a minor role within the first two channels. Moreover, with increasing cumulative strain, the predominant deformation mode in deformed grains shifted from basal <a> slip to prismatic <a> slip. The combined effects of segregation of solute atoms at recrystallized grain boundaries, SFs precipitation within recrystallized grains, and fragmented long-period stacking ordered (LPSO) phases effectively suppressed microstructural coarsening in the extruded sheets. The CADSE process represents a breakthrough in metal forming technology, establishing a new paradigm for anisotropic control and mechanical property enhancement. This innovative methodology establishes a general framework for extruded sheet manufacturing applicable across diverse material systems.
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来源期刊
Journal of Materials Processing Technology
Journal of Materials Processing Technology 工程技术-材料科学:综合
CiteScore
12.60
自引率
4.80%
发文量
403
审稿时长
29 days
期刊介绍: The Journal of Materials Processing Technology covers the processing techniques used in manufacturing components from metals and other materials. The journal aims to publish full research papers of original, significant and rigorous work and so to contribute to increased production efficiency and improved component performance. Areas of interest to the journal include: • Casting, forming and machining • Additive processing and joining technologies • The evolution of material properties under the specific conditions met in manufacturing processes • Surface engineering when it relates specifically to a manufacturing process • Design and behavior of equipment and tools.
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