基于仿真的超分辨率EBSD相对变形梯度张量测量

IF 2 3区 工程技术 Q2 MICROSCOPY
Aimo Winkelmann , Grzegorz Cios , Konrad Perzyński , Tomasz Tokarski , Klaus Mehnert , Łukasz Madej , Piotr Bała
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引用次数: 0

摘要

本文总结了一种电子背散射衍射(EBSD)的数据分析方法,该方法利用高分辨率菊池图模拟来测量实验测量的相对低分辨率菊池图的等时相对变形梯度张量。基于模拟的理论测试衍射图的超采样使得从低分辨率实验图中获得的应变和方向的最佳拟合确定中获得的张量参数的精度得到显著提高。作为一个应用,我们展示了高分辨率的取向和应变分析模型案例的硬度测试压痕在硅(100)晶圆上,使用变分辨率菊池图案。该方法表明,在硅片的名义上无应变区域的相对偏应变范数和相对旋转角度中,噪声水平接近1×10−4。应变和旋转测量由有限元模拟解释。虽然证实了以前发表的研究的基本发现,但目前的方法可以将必要的模式数据大小减少大约两个数量级。我们估计,256 × 256像素的模式分辨率应该足以解决大多数使用模式匹配技术的EBSD分析任务。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Simulation-based super-resolution EBSD for measurements of relative deformation gradient tensors
We summarize a data analysis approach for electron backscatter diffraction (EBSD) which uses high-resolution Kikuchi pattern simulations to measure isochoric relative deformation gradient tensors from experimentally measured Kikuchi patterns of relatively low resolution. Simulation-based supersampling of the theoretical test diffraction patterns enables a significant precision improvement of tensor parameters obtained in best-fit determinations of strains and orientations from low-resolution experimental patterns. As an application, we demonstrate high-resolution orientation and strain analysis for the model case of hardness test indents on a Si(100) wafer, using Kikuchi patterns of variable resolution. The approach shows noise levels near 1×104 in the relative deviatoric strain norm and in the relative rotation angles on nominally strain-free regions of the silicon wafer. The strain and rotation measurements are interpreted by finite element simulations. While confirming the basic findings of previously published studies, the present approach enables a potential reduction in the necessary pattern data size by about two orders of magnitude. We estimate that pattern resolutions in the order of 256 × 256 pixels should be enough to solve a majority of EBSD analysis tasks using pattern matching techniques.
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来源期刊
Ultramicroscopy
Ultramicroscopy 工程技术-显微镜技术
CiteScore
4.60
自引率
13.60%
发文量
117
审稿时长
5.3 months
期刊介绍: Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.
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