Benjamin Dassonneville, Heiner Detert, Dieter Schollmeyer
{"title":"(3 z) 4-methyl-9 - (4-methyl-benzene-sulfon-yl) -N-phenyl-3H 9 h-thio-pyrano indol-3-imine(3、4 b)。","authors":"Benjamin Dassonneville, Heiner Detert, Dieter Schollmeyer","doi":"10.1107/S2414314625004754","DOIUrl":null,"url":null,"abstract":"<p><p>The title indolothiopyrane imine, C<sub>25</sub>H<sub>20</sub>N<sub>2</sub>O<sub>2</sub>S<sub>2</sub>, which was prepared by a [2 + 2 + 2] cycloaddition reaction, crystallizes with two molecules in the asymmetric unit. Both adopt the shape of a staircase with two steps, consolidated by intramolecular C-H⋯O interactions.</p>","PeriodicalId":94324,"journal":{"name":"IUCrData","volume":"10 Pt 5","pages":"x250475"},"PeriodicalIF":0.0000,"publicationDate":"2025-05-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12142394/pdf/","citationCount":"0","resultStr":"{\"title\":\"(3<i>Z</i>)-4-Methyl-9-(4-methyl-benzene-sulfon-yl)-<i>N</i>-phenyl-3<i>H</i>,9<i>H</i>-thio-pyrano[3,4-<i>b</i>]indol-3-imine.\",\"authors\":\"Benjamin Dassonneville, Heiner Detert, Dieter Schollmeyer\",\"doi\":\"10.1107/S2414314625004754\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>The title indolothiopyrane imine, C<sub>25</sub>H<sub>20</sub>N<sub>2</sub>O<sub>2</sub>S<sub>2</sub>, which was prepared by a [2 + 2 + 2] cycloaddition reaction, crystallizes with two molecules in the asymmetric unit. Both adopt the shape of a staircase with two steps, consolidated by intramolecular C-H⋯O interactions.</p>\",\"PeriodicalId\":94324,\"journal\":{\"name\":\"IUCrData\",\"volume\":\"10 Pt 5\",\"pages\":\"x250475\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2025-05-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12142394/pdf/\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"IUCrData\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1107/S2414314625004754\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2025/5/1 0:00:00\",\"PubModel\":\"eCollection\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"IUCrData","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1107/S2414314625004754","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2025/5/1 0:00:00","PubModel":"eCollection","JCR":"","JCRName":"","Score":null,"Total":0}
The title indolothiopyrane imine, C25H20N2O2S2, which was prepared by a [2 + 2 + 2] cycloaddition reaction, crystallizes with two molecules in the asymmetric unit. Both adopt the shape of a staircase with two steps, consolidated by intramolecular C-H⋯O interactions.
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