无磁场电子显微镜成像系统的研制

IF 2 3区 工程技术 Q2 MICROSCOPY
T. Maekawa , Y. Kohno , A. Yasuhara , S. Morishita , T. Inoue , Y. Ueda , K. Arakawa
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引用次数: 0

摘要

用于高分辨率成像的无磁场物镜的成功开发使得在样品周围无磁场条件下获得原子分辨率扫描透射电子显微镜(STEM)图像成为可能。利用这种无磁场物镜进行常规透射电子显微镜(TEM)观察有望为磁性材料的全面表征提供优势。这种方法在现场观测中特别重要。为了获得常规的TEM图像,如明暗场图像,重要的是将物镜孔径定位在衍射平面上,通常是物镜的后焦平面。然而,对于无磁场物镜,将物镜孔径定位在被多个磁极包围的后焦平面周围是不可行的。在本研究中,我们描述了一种成像系统的发展,该系统可以将孔径定位在与后焦平面共轭的衍射平面上。此外,用于无磁场物镜的宽间隙极片的开发使得使用具有厚尖端的样品支架进行原位观测成为可能。无磁场电子显微镜集成了新开发的极片和图像形成系统以及高阶像差校正器,不仅提供原子分辨率的TEM/STEM观测,而且还提供了在无磁场环境中表征磁性材料的通用方法。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Development of an image-forming system for the magnetic field-free electron microscope
The successful development of a magnetic field-free objective lens for high-resolution imaging has enabled the acquisition of atomic-resolution scanning transmission electron microscopy (STEM) images under magnetic field-free conditions around the sample. Utilizing this magnetic field-free objective lens for conventional transmission electron microscopy (TEM) observations is expected to offer advantages for the comprehensive characterization of magnetic materials. This approach is particularly significant in the context of in-situ observations. To obtain conventional TEM images, such as bright- and dark-field images, it is important to position the objective lens aperture in a diffraction plane, typically the back focal plane of the objective lens. However, positioning the objective lens aperture around the back focal plane, which is surrounded by multiple magnetic poles, is not feasible for the magnetic field-free objective lens. In this study, we describe the development of an image-forming system that can position the aperture in a diffraction plane conjugate to the back focal plane. In addition, the development of a wide-gap pole piece for the magnetic field-free objective lens has enabled the use of sample holders with thick tips for in-situ observations. The magnetic field-free electron microscope, which integrates a newly developed pole piece and image-forming system with higher-order aberration correctors, offers not only atomic-resolution TEM/STEM observations but also a versatile approach for the characterization of magnetic materials in a magnetic field-free environment.
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来源期刊
Ultramicroscopy
Ultramicroscopy 工程技术-显微镜技术
CiteScore
4.60
自引率
13.60%
发文量
117
审稿时长
5.3 months
期刊介绍: Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.
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