不同表面处理对氧化锆结合强度的影响。

IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE
Kushaldeep Fnu, Leen Musharbash, Fusun Ozer, Francis Mante, Julian Conejo, Viram Upadhyaya, Eva Anadioti, Markus B Blatz
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引用次数: 0

摘要

目的:评价不同表面处理方法对氧化锆与基体结合强度的影响。材料与方法:烧结二氧化锆陶瓷盘(KATANA Zirconia STML;N = 20;尺寸为12 × 12 × 3 mm),分为五组:未表面处理组(C组)、50µm氧化铝研磨空气粒子组(AA组)、玻璃微珠研磨空气粒子组(GB组)、锆E蚀刻液2 h (ZE组)、48%氢氟酸溶液25℃加热30 min (HE组)。圆柱形复合树脂试件(直径2.1 mm,高3mm)在1000 g载荷下用树脂水泥(Panavia V5)与氧化锆试件粘接,光固化80 s。每组分为两组,37℃蒸馏水中保存24 h或10000次热循环后,以1 mm/min的十字头速度测试剪切粘结强度(SBS)。在立体显微镜下观察试样的断裂面,并将其破坏模式分为粘接破坏、内聚破坏和混合破坏。采用单因素方差分析和配对t检验进行统计分析。结果:AA组SBS平均值最高(14.98±3.19),其次为HF组(14.8±0.83)、C组(8.32±1.95)、GB组(9.29±0.99)、ZE组(4.83±0.47)。热循环后各组平均SBS值(MPa)均显著降低,分别为5.45±0.8 (C组)、13.47±2.33 (AA组)、8.56±1.35 (GB组)、4.16±0.63 (ZE组)、13.15±1.27 (HF组)。结论:氧化铝和加热48%氢氟酸的空气颗粒磨损比其他表面处理具有更高的结合强度。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The effect of different surface treatments on the bond strength to zirconia.

Purpose: To evaluate the effect of various surface treatment methods on zirconia as it affects the bond strength to its substrate.

Materials and methods: Sintered zirconium dioxide ceramic disks (KATANA Zirconia STML; n = 20; size 12 × 12 × 3 mm) were divided into five groups: no surface treatment (Group C), air-particle abraded with 50 µm aluminum oxide (Group AA), air-particle abraded with glass beads (Group GB), Zircos E etching solution for 2 h (Group ZE), and 48% hydrofluoric acid solution heated at 25°C for 30 min (Group HE). Cylindrical composite resin specimens (2.1 mm in diameter, 3 mm in height) were bonded to the zirconia samples with resin cement (Panavia V5) under a load of 1000 g and light cured for 80 s. Each group was divided into two subgroups, and shear bond strength (SBS) was tested at a crosshead speed of 1 mm/min after storage in distilled water for 24 h at 37°C or after 10,000 thermocycles. The fractured surfaces of specimens were inspected with a stereo microscope, and failure modes were classified as adhesive, cohesive, or mixed failures. One-way ANOVA test and paired t-test were applied for statistical analysis.

Results: Highest mean SBS values [MPa] were observed for Group AA (14.98 ± 3.19) followed by Group HF (14.8 ± 0.83), Group C (8.32  ± 1.95), Group GB (9.29 ± 0.99), and Group ZE (4.83 ± 0.47). Mean SBS values (MPa) of all the groups decreased significantly after thermal cycling and were for 5.45 ± 0.8 (Group C), 13.47 ± 2.33 (Group AA), 8.56 ± 1.35 (Group GB), 4.16 ± 0.63 (Group ZE), and 13.15 ± 1.27 (Group HF).

Conclusions: Air-particle abrasion with alumina and heated 48% hydrofluoric acid provide higher bond strengths than the other surface treatments tested.

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来源期刊
CiteScore
7.90
自引率
15.00%
发文量
171
审稿时长
6-12 weeks
期刊介绍: The Journal of Prosthodontics promotes the advanced study and practice of prosthodontics, implant, esthetic, and reconstructive dentistry. It is the official journal of the American College of Prosthodontists, the American Dental Association-recognized voice of the Specialty of Prosthodontics. The journal publishes evidence-based original scientific articles presenting information that is relevant and useful to prosthodontists. Additionally, it publishes reports of innovative techniques, new instructional methodologies, and instructive clinical reports with an interdisciplinary flair. The journal is particularly focused on promoting the study and use of cutting-edge technology and positioning prosthodontists as the early-adopters of new technology in the dental community.
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