Bo Li , Xiuyu Yu , Zhicheng Huang , Zhaojie Chu , Han Yang , Qinyi Zhu , Xicong Ye , Dong Fang , Youlu Yuan
{"title":"FeCoCrNiAl0.1高熵合金热变形表征:三维加工图、有限元数值模拟和显微组织演变","authors":"Bo Li , Xiuyu Yu , Zhicheng Huang , Zhaojie Chu , Han Yang , Qinyi Zhu , Xicong Ye , Dong Fang , Youlu Yuan","doi":"10.1016/j.intermet.2025.108821","DOIUrl":null,"url":null,"abstract":"<div><div>To investigate the hot deformation and dynamic recrystallization (DRX) behavior of FeCoCrNiAl<sub>0.1</sub> high-entropy alloy (HEA), hot compression tests were conducted under varying temperatures range of 950–1100 °C with strain rates range of 0.001 and 1 s<sup>−1</sup>. FeCoCrNiAl<sub>0.1</sub> HEA exhibit distinct DRX characteristics, synergistically controlled by dynamic recovery (DRV) and DRX. The hot processing map indicates that the studied alloy exhibits an optimal hot processing window of 1000–1100 °C/0.001–0.02 s<sup>−1</sup>. According to finite element model (FEM), DRX distribution is temperature and strain-rate-dependent. The DRX region expands radially from core to peripheral with increasing temperature or decreasing strain rate. Microstructural evolution analysis reveals that the studied alloy exhibits pronounced DRV and DRX characteristics during hot deformation. DRX primarily proceeds through Continuous Dynamic Recrystallization (CDRX) driven by subgrain rotation and Discontinuous Dynamic Recrystallization (DDRX) through grain boundary bulging nucleation. As strain rate decreases or temperature increases, the studied alloy exhibits a grain coarsening and substantial dislocation density reduction. The grain orientation evolves from the typical R texture {134}<211> to the Cube texture {001}<100>, and this texture transition facilitates the progression of DRX.</div></div>","PeriodicalId":331,"journal":{"name":"Intermetallics","volume":"183 ","pages":"Article 108821"},"PeriodicalIF":4.3000,"publicationDate":"2025-05-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Characterization of hot deformation of FeCoCrNiAl0.1 high entropy alloy: 3D processing maps, FEM numerical simulation and microstructure evolution\",\"authors\":\"Bo Li , Xiuyu Yu , Zhicheng Huang , Zhaojie Chu , Han Yang , Qinyi Zhu , Xicong Ye , Dong Fang , Youlu Yuan\",\"doi\":\"10.1016/j.intermet.2025.108821\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>To investigate the hot deformation and dynamic recrystallization (DRX) behavior of FeCoCrNiAl<sub>0.1</sub> high-entropy alloy (HEA), hot compression tests were conducted under varying temperatures range of 950–1100 °C with strain rates range of 0.001 and 1 s<sup>−1</sup>. FeCoCrNiAl<sub>0.1</sub> HEA exhibit distinct DRX characteristics, synergistically controlled by dynamic recovery (DRV) and DRX. The hot processing map indicates that the studied alloy exhibits an optimal hot processing window of 1000–1100 °C/0.001–0.02 s<sup>−1</sup>. According to finite element model (FEM), DRX distribution is temperature and strain-rate-dependent. The DRX region expands radially from core to peripheral with increasing temperature or decreasing strain rate. Microstructural evolution analysis reveals that the studied alloy exhibits pronounced DRV and DRX characteristics during hot deformation. DRX primarily proceeds through Continuous Dynamic Recrystallization (CDRX) driven by subgrain rotation and Discontinuous Dynamic Recrystallization (DDRX) through grain boundary bulging nucleation. As strain rate decreases or temperature increases, the studied alloy exhibits a grain coarsening and substantial dislocation density reduction. The grain orientation evolves from the typical R texture {134}<211> to the Cube texture {001}<100>, and this texture transition facilitates the progression of DRX.</div></div>\",\"PeriodicalId\":331,\"journal\":{\"name\":\"Intermetallics\",\"volume\":\"183 \",\"pages\":\"Article 108821\"},\"PeriodicalIF\":4.3000,\"publicationDate\":\"2025-05-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Intermetallics\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0966979525001864\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, PHYSICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Intermetallics","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0966979525001864","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, PHYSICAL","Score":null,"Total":0}
Characterization of hot deformation of FeCoCrNiAl0.1 high entropy alloy: 3D processing maps, FEM numerical simulation and microstructure evolution
To investigate the hot deformation and dynamic recrystallization (DRX) behavior of FeCoCrNiAl0.1 high-entropy alloy (HEA), hot compression tests were conducted under varying temperatures range of 950–1100 °C with strain rates range of 0.001 and 1 s−1. FeCoCrNiAl0.1 HEA exhibit distinct DRX characteristics, synergistically controlled by dynamic recovery (DRV) and DRX. The hot processing map indicates that the studied alloy exhibits an optimal hot processing window of 1000–1100 °C/0.001–0.02 s−1. According to finite element model (FEM), DRX distribution is temperature and strain-rate-dependent. The DRX region expands radially from core to peripheral with increasing temperature or decreasing strain rate. Microstructural evolution analysis reveals that the studied alloy exhibits pronounced DRV and DRX characteristics during hot deformation. DRX primarily proceeds through Continuous Dynamic Recrystallization (CDRX) driven by subgrain rotation and Discontinuous Dynamic Recrystallization (DDRX) through grain boundary bulging nucleation. As strain rate decreases or temperature increases, the studied alloy exhibits a grain coarsening and substantial dislocation density reduction. The grain orientation evolves from the typical R texture {134}<211> to the Cube texture {001}<100>, and this texture transition facilitates the progression of DRX.
期刊介绍:
This journal is a platform for publishing innovative research and overviews for advancing our understanding of the structure, property, and functionality of complex metallic alloys, including intermetallics, metallic glasses, and high entropy alloys.
The journal reports the science and engineering of metallic materials in the following aspects:
Theories and experiments which address the relationship between property and structure in all length scales.
Physical modeling and numerical simulations which provide a comprehensive understanding of experimental observations.
Stimulated methodologies to characterize the structure and chemistry of materials that correlate the properties.
Technological applications resulting from the understanding of property-structure relationship in materials.
Novel and cutting-edge results warranting rapid communication.
The journal also publishes special issues on selected topics and overviews by invitation only.