Min Zhang , Shuai Dong , Zihao Li , Kesen Zhao , Aile Wang , Wenjie Meng , Qiyuan Feng , Jing Zhang , Jihao Wang , Yalin Lu , Yubin Hou , Qingyou Lu
{"title":"在12 T超导磁体上的原位±90°可旋转磁力显微镜的紧凑设计,构建和评估","authors":"Min Zhang , Shuai Dong , Zihao Li , Kesen Zhao , Aile Wang , Wenjie Meng , Qiyuan Feng , Jing Zhang , Jihao Wang , Yalin Lu , Yubin Hou , Qingyou Lu","doi":"10.1016/j.ultramic.2025.114155","DOIUrl":null,"url":null,"abstract":"<div><div>Cryogenic magnetic force microscopy (MFM) is a powerful technique capable of resolving exotic magnetic textures with nanoscale resolution in real-space. We introduce a cryogenic rotatable MFM (CRMFM) that enables the visualization of in situ evolution of magnetic domains by rotating magnetic samples between −90° and +90° within a 12 T superconducting magnet. By continuously rotating the sample under an external magnetic field, the direction of the magnetic field can be varied from out-of-plane to in-plane, enabling microscopic analysis experiments that require vector magnetic fields within the CRMFM system. By using CRMFM measurements, we successfully transformed long magnetic stripe domains into isolated magnetic bubble domains and proposed a novel strategy for visualizing stripe-bubble transitions in magnetic domains. Additionally, we demonstrated that the CRMFM system can generate high-quality MFM images under in-plane magnetic fields up to 12 T. Our research provides a framework for visualizing the interaction between ferromagnetism and magnetic field direction, facilitating the study of magnetic crystal anisotropy.</div></div>","PeriodicalId":23439,"journal":{"name":"Ultramicroscopy","volume":"274 ","pages":"Article 114155"},"PeriodicalIF":2.0000,"publicationDate":"2025-05-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Compact design, construction, and evaluation of an in situ ±90° rotatable magnetic force microscope in a 12 T superconducting magnet\",\"authors\":\"Min Zhang , Shuai Dong , Zihao Li , Kesen Zhao , Aile Wang , Wenjie Meng , Qiyuan Feng , Jing Zhang , Jihao Wang , Yalin Lu , Yubin Hou , Qingyou Lu\",\"doi\":\"10.1016/j.ultramic.2025.114155\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Cryogenic magnetic force microscopy (MFM) is a powerful technique capable of resolving exotic magnetic textures with nanoscale resolution in real-space. We introduce a cryogenic rotatable MFM (CRMFM) that enables the visualization of in situ evolution of magnetic domains by rotating magnetic samples between −90° and +90° within a 12 T superconducting magnet. By continuously rotating the sample under an external magnetic field, the direction of the magnetic field can be varied from out-of-plane to in-plane, enabling microscopic analysis experiments that require vector magnetic fields within the CRMFM system. By using CRMFM measurements, we successfully transformed long magnetic stripe domains into isolated magnetic bubble domains and proposed a novel strategy for visualizing stripe-bubble transitions in magnetic domains. Additionally, we demonstrated that the CRMFM system can generate high-quality MFM images under in-plane magnetic fields up to 12 T. Our research provides a framework for visualizing the interaction between ferromagnetism and magnetic field direction, facilitating the study of magnetic crystal anisotropy.</div></div>\",\"PeriodicalId\":23439,\"journal\":{\"name\":\"Ultramicroscopy\",\"volume\":\"274 \",\"pages\":\"Article 114155\"},\"PeriodicalIF\":2.0000,\"publicationDate\":\"2025-05-03\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Ultramicroscopy\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0304399125000543\",\"RegionNum\":3,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MICROSCOPY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Ultramicroscopy","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0304399125000543","RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MICROSCOPY","Score":null,"Total":0}
Compact design, construction, and evaluation of an in situ ±90° rotatable magnetic force microscope in a 12 T superconducting magnet
Cryogenic magnetic force microscopy (MFM) is a powerful technique capable of resolving exotic magnetic textures with nanoscale resolution in real-space. We introduce a cryogenic rotatable MFM (CRMFM) that enables the visualization of in situ evolution of magnetic domains by rotating magnetic samples between −90° and +90° within a 12 T superconducting magnet. By continuously rotating the sample under an external magnetic field, the direction of the magnetic field can be varied from out-of-plane to in-plane, enabling microscopic analysis experiments that require vector magnetic fields within the CRMFM system. By using CRMFM measurements, we successfully transformed long magnetic stripe domains into isolated magnetic bubble domains and proposed a novel strategy for visualizing stripe-bubble transitions in magnetic domains. Additionally, we demonstrated that the CRMFM system can generate high-quality MFM images under in-plane magnetic fields up to 12 T. Our research provides a framework for visualizing the interaction between ferromagnetism and magnetic field direction, facilitating the study of magnetic crystal anisotropy.
期刊介绍:
Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.