通过低聚苯基氧化物自由基光氧化还原催化卤代酚与偶氮的亲核芳香取代

IF 15.6 1区 化学 Q1 CHEMISTRY, MULTIDISCIPLINARY
Jan Seliger, Lydia R. Fries, Jonathan M. Meinhardt and Robert R. Knowles*, 
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引用次数: 0

摘要

亲核芳香取代(SNAr)反应广泛应用于有机合成,但通常需要使用缺电子芳烃来提高反应活性。在此,我们报道了一种在温和的氧化还原中性条件下,富电子4-卤代酚与唑类亲核试剂形成形式SNAr的光催化方案。该转化通过两个阶段的机制进行,包括最初的卤代酚寡聚产生一个关键的低聚物(苯基氧化物)中间体,随后通过SNAr与光氧化还原催化的芳烃混合使之成为可能。反应监测、化学计量控制实验和发光猝灭数据表明,苯氧基自由基和Brønsted酸激活的低聚(苯基氧化苯)自由基分别是低聚和SNAr阶段的反应物质。该方法在17种(伪)含各种离去基(F、Cl、Br、OMs和OTs)的卤代酚和22种唑类化合物中得到了证明。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Photoredox-Catalyzed Nucleophilic Aromatic Substitution of Halophenols with Azoles via Oligomeric Phenylene Oxide Radicals

Photoredox-Catalyzed Nucleophilic Aromatic Substitution of Halophenols with Azoles via Oligomeric Phenylene Oxide Radicals

Nucleophilic aromatic substitution (SNAr) reactions are widely employed in organic synthesis yet typically require the use of electron-deficient arenes for efficient reactivity. Herein, we report a photocatalytic protocol for formal SNAr of electron-rich 4-halophenols with azole nucleophiles under mild, redox-neutral conditions. The transformation proceeds via a two-stage mechanism consisting of initial halophenol oligomerization to produce a key oligo(phenylene oxide) intermediate and its subsequent breakdown through SNAr with the azole enabled by photoredox-catalyzed arene umpolung. Reaction monitoring, stoichiometric control experiments, and luminescence quenching data implicate phenoxyl radicals and Brønsted acid-activated oligo(phenylene oxide) radicals as the reactive species in the oligomerization and the SNAr stages, respectively. The synthetic utility of this method is demonstrated across 17 (pseudo)halophenols bearing a variety of leaving groups (F, Cl, Br, OMs, and OTs) and 22 azole examples.

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来源期刊
CiteScore
24.40
自引率
6.00%
发文量
2398
审稿时长
1.6 months
期刊介绍: The flagship journal of the American Chemical Society, known as the Journal of the American Chemical Society (JACS), has been a prestigious publication since its establishment in 1879. It holds a preeminent position in the field of chemistry and related interdisciplinary sciences. JACS is committed to disseminating cutting-edge research papers, covering a wide range of topics, and encompasses approximately 19,000 pages of Articles, Communications, and Perspectives annually. With a weekly publication frequency, JACS plays a vital role in advancing the field of chemistry by providing essential research.
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