Lubabalo Ndima , Eric Cyriel Hosten , Richard Betz
{"title":"四苯基乙醇酸四氢呋喃单溶剂化物。","authors":"Lubabalo Ndima , Eric Cyriel Hosten , Richard Betz","doi":"10.1107/S2414314624012410","DOIUrl":null,"url":null,"abstract":"<div><div>The title compound is the symmetric glycolide derived from benzilic acid featuring a disordered tetrahydrofuran solvent molecule in the crystal structure.</div></div><div><div>The title compound, C<sub>28</sub>H<sub>20</sub>O<sub>4</sub>·C<sub>4</sub>H<sub>4</sub>O, is the cyclic ester anhydride of benzilic acid. A disordered solvent molecule is present in the structure. The asymmetric unit contains half the acid-derived molecule. C—H⋯O contacts connect the constituents of the title compound into a three-dimensional network.<span><figure><span><img><ol><li><span><span>Download: <span>Download high-res image (250KB)</span></span></span></li><li><span><span>Download: <span>Download full-size image</span></span></span></li></ol></span></figure></span></div></div>","PeriodicalId":94324,"journal":{"name":"IUCrData","volume":"10 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11799779/pdf/","citationCount":"0","resultStr":"{\"title\":\"Tetraphenylglycolide tetrahydrofuran monosolvate\",\"authors\":\"Lubabalo Ndima , Eric Cyriel Hosten , Richard Betz\",\"doi\":\"10.1107/S2414314624012410\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The title compound is the symmetric glycolide derived from benzilic acid featuring a disordered tetrahydrofuran solvent molecule in the crystal structure.</div></div><div><div>The title compound, C<sub>28</sub>H<sub>20</sub>O<sub>4</sub>·C<sub>4</sub>H<sub>4</sub>O, is the cyclic ester anhydride of benzilic acid. A disordered solvent molecule is present in the structure. The asymmetric unit contains half the acid-derived molecule. C—H⋯O contacts connect the constituents of the title compound into a three-dimensional network.<span><figure><span><img><ol><li><span><span>Download: <span>Download high-res image (250KB)</span></span></span></li><li><span><span>Download: <span>Download full-size image</span></span></span></li></ol></span></figure></span></div></div>\",\"PeriodicalId\":94324,\"journal\":{\"name\":\"IUCrData\",\"volume\":\"10 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2025-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11799779/pdf/\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"IUCrData\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/org/science/article/pii/S241431462500001X\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"IUCrData","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/org/science/article/pii/S241431462500001X","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
The title compound is the symmetric glycolide derived from benzilic acid featuring a disordered tetrahydrofuran solvent molecule in the crystal structure.
The title compound, C28H20O4·C4H4O, is the cyclic ester anhydride of benzilic acid. A disordered solvent molecule is present in the structure. The asymmetric unit contains half the acid-derived molecule. C—H⋯O contacts connect the constituents of the title compound into a three-dimensional network.