S. A. Bobuyok, A. P. Surzhikov, E. V. Nikolaev, A. V. Malyshev, E. N. Lysenko
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引用次数: 0
摘要
我们利用热磁分析和记录初始磁导率\({{\mu }_{0}}\left( T \right)\)和比电阻率\(\rho \left( T \right)\)与温度的关系的方法,研究了成分为\({\text{N}}{{{\text{i}}}_{{0.4}}}{\text{Z}}{{{\text{n}}}_{{0.6}}}{\text{F}}{{{\text{e}}}_{2}}{{{\text{O}}}_{4}}\)的铁氧体材料在居里温度附近的磁相变。该研究对所使用的设备和所考虑的实验方法的关键特征进行了描述。在冷却阶段的热磁分析中,发现材料完成向铁磁态转变的温度对应于\({{\mu }_{0}}\left( T \right)\)曲线上的拐点和\(\ln \rho \left( T \right)\)依赖图上的断点。建立的转变过程参数间的相互作用有助于更精确地测定铁氧体中的居里温度。
Comparative Analysis of Experimental Methods for Determining the Curie Temperature of Ferrite Materials
We studied magnetic phase transitions near the Curie temperature in the ferrite material with the composition \({\text{N}}{{{\text{i}}}_{{0.4}}}{\text{Z}}{{{\text{n}}}_{{0.6}}}{\text{F}}{{{\text{e}}}_{2}}{{{\text{O}}}_{4}}\) using thermomagnetometric analysis and methods for recording the temperature dependences of initial magnetic permeability \({{\mu }_{0}}\left( T \right)\) and specific electrical resistivity \(\rho \left( T \right)\). The study provides a description of the equipment used and the key features of the experimental methods under consideration. During thermomagnetometric analysis in the cooling phase, it has been found that the temperature at which the material completes its transition to the ferrimagnetic state corresponds to the inflection point on the \({{\mu }_{0}}\left( T \right)\) curve and the break point on the \(\ln \rho \left( T \right)\) dependence graph. The established interaction between the parameters of transition processes may be useful for more accurate determination of the Curie temperature in ferrites.
期刊介绍:
Russian Journal of Nondestructive Testing, a translation of Defectoskopiya, is a publication of the Russian Academy of Sciences. This publication offers current Russian research on the theory and technology of nondestructive testing of materials and components. It describes laboratory and industrial investigations of devices and instrumentation and provides reviews of new equipment developed for series manufacture. Articles cover all physical methods of nondestructive testing, including magnetic and electrical; ultrasonic; X-ray and Y-ray; capillary; liquid (color luminescence), and radio (for materials of low conductivity).