——2,4-Di-chloro-6 N - [2 - (tri-fluoro-meth-yl) phen-yl] carboximido-yl phenol…….

IUCrData Pub Date : 2024-11-01 DOI:10.1107/S2414314624010745

Zizipho Xantini , Alfred Muller , Koop Lammertsma

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引用次数: 0

摘要

标题化合物C14H8Cl2F3NO由三氟甲基苯胺与二氯水杨醛亲核加成缩合成半胺，脱水生成亚胺。该化合物在两个芳环之间形成一个二面角为44.70(5)°的正菱形Pbca （Z = 8）空间群。在晶体中，分子聚集在一起，沿着c轴形成之字形图案。

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2,4-Dichloro-6-{N-[2-(trifluoromethyl)phenyl]carboximidoyl}phenol

The title compound was synthesized by the condensation between trifluoromethylaniline and dichlorosalicylaldehyde by nucleophilic addition, forming a hemiaminal, followed by a dehydration to generate an imine. The compound crystallizes in an orthorhombic Pbca (Z = 8) space group with a dihedral angle of 44.70 (5)° between the two aromatic rings. In the crystal, the molecules pack together to form a zigzag pattern along the c axis.

The title compound, C₁₄H₈Cl₂F₃NO, was synthesized by the condensation between trifluoromethylaniline and dichlorosalicylaldehyde by nucleophilic addition, forming a hemiaminal, followed by a dehydration to generate an imine. The compound crystallizes in an orthorhombic Pbca (Z = 8) space group with a dihedral angle of 44.70 (5)° between the two aromatic rings. In the crystal, the molecules pack together to form a zigzag pattern along the c axis.

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IUCrData

CiteScore

0.30

自引率

0.00%

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