基于钕2O3/石墨烯的高灵敏度电化学传感器用于监测棕榈油产品中的添加剂化合物

IF 4.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Rahmat Hidayat , Ganjar Fadillah , Febi Indah Fajarwati , Aldo Diandra Nur Ramdani , Qonita Awliya Hanif , Muhaimin
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引用次数: 0

摘要

在棕榈油产品中使用 3-氯丙二醇(3-MCPDs)等添加剂会影响产品质量和安全。因此,灵敏而准确的检测方法至关重要。本研究探讨了 Nd₂O₃/石墨烯(Nd₂O₃/G)复合材料的水热合成及其作为电化学传感器的应用,以检测棕榈油产品中作为添加剂化合物的 3-MCPD。傅立叶变换红外(FTIR)、X 射线衍射(XRD)和扫描电子显微镜(SEM)等不同的表征技术为 Nd₂O₃/G 复合材料的成功组装和正排列提供了证据。在检测棕榈油中的典型添加剂(3-MCPDs)方面,对传感器的电化学功效进行了评估。传感器性能测试采用伏安技术进行研究。改进后的传感器在检测 3-MCPDs 方面表现出良好的分析性能,电催化活性、电子传递和电荷转移电阻(Rct)均有所提高。这些改进大大提高了传感器准确检测 3-MCPDs 的能力,其检测限为 0.65 μM。这种新开发的传感器具有极高的稳定性和准确性,因此有望应用于质量控制和日常分析过程中。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Highly sensitive electrochemical sensor based Nd2O3/graphene for monitoring additive compounds in palm oil product
The use of additives, such as 3-monochloropropane-1,2-diol (3-MCPDs), in palm oil products can impact the product's quality and safety. Therefore, it is essential to have a sensitive and accurate detection method. This study explored the hydrothermal synthesis of Nd₂O₃/graphene (Nd₂O₃/G) composites and their application as electrochemical sensors for detecting 3-MCPDs as additive compounds in palm oil products. Different techniques for characterization, such as Fourier Transform Infra-Red (FTIR), X-ray diffraction (XRD), and Scanning Electron Microscopy (SEM), supply evidence supporting the successful assembly and positive arrangement of the Nd₂O₃/G composite. The sensor's electrochemical efficacy is assessed concerning the detection of typical additives found in palm oil (3-MCPDs). The sensor performance test is studied by voltammetric technique. The modified sensor showed good analytical performance for detection of 3-MCPDs with improving electrocatalytic activity, electron transfer, and reduced charge transfer resistance (Rct). These modifications greatly enhance the sensor's ability to accurately detect 3-MCPDs with limit of detection of 0.65 μM. This developed sensor shows a great stability and accuracy, thus it has potential to apply in quality control and daily analysis process.
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来源期刊
Materials Chemistry and Physics
Materials Chemistry and Physics 工程技术-材料科学:综合
CiteScore
8.70
自引率
4.30%
发文量
1515
审稿时长
69 days
期刊介绍: Materials Chemistry and Physics is devoted to short communications, full-length research papers and feature articles on interrelationships among structure, properties, processing and performance of materials. The Editors welcome manuscripts on thin films, surface and interface science, materials degradation and reliability, metallurgy, semiconductors and optoelectronic materials, fine ceramics, magnetics, superconductors, specialty polymers, nano-materials and composite materials.
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