{"title":"通过直接粉末锻造制造的粉末状铁铝化物 Fe - 28Al 的机械性能","authors":"Oleksandr Tolochyn, Oleksandra Tolochyna, Gennadii Bagliuk, Yan Yevych, Vitalii Danylenko, Yury Podrezov","doi":"10.1016/j.intermet.2024.108537","DOIUrl":null,"url":null,"abstract":"<div><div>This study examines the impact of direct powder forging of powders on the composition, structure, and mechanical properties of iron aluminide Fe–28 at. % Al. During the synthesis and forging of Fe<sub>3</sub>Al powders, a homogeneous A2 phase is formed at a temperature of 1100 °C. Porosity after forging is 2–2.5 %. Residual pores are predominantly planar in shape and are located at the boundaries of the powder particles. Annealing at 1300 °C improves the quality of interparticle boundaries and all samples exhibit transcrystalline fracture mechanism. Samples forged at 1100 °C and annealed at 1300 °C show maximum strength σ<sub>bend</sub> = 1050 MPa and fracture toughness K<sub>1c</sub> = 32.3 MPa·m<sup>1/2</sup>. The yield strength demonstrates anomalous temperature sensitivity with a maximum of 400 °C and at 500 °C. Samples tested at 600 °C show a decrease in yield strength, but a high enough yield point σ<sub>y</sub> ∼400 MPa and a high strengthening rate are very important for high-temperature creep resistance. In creep experiments at a load of 120 MPa at 600 °C, the strain rate varies in the range of 10<sup>−7</sup>–10<sup>−6</sup> s<sup>−1</sup>, the value of the rate sensitivity n ≈ 4. The main mechanism of creep is dislocation glide.</div></div>","PeriodicalId":331,"journal":{"name":"Intermetallics","volume":"175 ","pages":"Article 108537"},"PeriodicalIF":4.3000,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Mechanical behavior of powdered iron aluminide Fe – 28Al manufactured by direct powder forging\",\"authors\":\"Oleksandr Tolochyn, Oleksandra Tolochyna, Gennadii Bagliuk, Yan Yevych, Vitalii Danylenko, Yury Podrezov\",\"doi\":\"10.1016/j.intermet.2024.108537\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>This study examines the impact of direct powder forging of powders on the composition, structure, and mechanical properties of iron aluminide Fe–28 at. % Al. During the synthesis and forging of Fe<sub>3</sub>Al powders, a homogeneous A2 phase is formed at a temperature of 1100 °C. Porosity after forging is 2–2.5 %. Residual pores are predominantly planar in shape and are located at the boundaries of the powder particles. Annealing at 1300 °C improves the quality of interparticle boundaries and all samples exhibit transcrystalline fracture mechanism. Samples forged at 1100 °C and annealed at 1300 °C show maximum strength σ<sub>bend</sub> = 1050 MPa and fracture toughness K<sub>1c</sub> = 32.3 MPa·m<sup>1/2</sup>. The yield strength demonstrates anomalous temperature sensitivity with a maximum of 400 °C and at 500 °C. Samples tested at 600 °C show a decrease in yield strength, but a high enough yield point σ<sub>y</sub> ∼400 MPa and a high strengthening rate are very important for high-temperature creep resistance. In creep experiments at a load of 120 MPa at 600 °C, the strain rate varies in the range of 10<sup>−7</sup>–10<sup>−6</sup> s<sup>−1</sup>, the value of the rate sensitivity n ≈ 4. The main mechanism of creep is dislocation glide.</div></div>\",\"PeriodicalId\":331,\"journal\":{\"name\":\"Intermetallics\",\"volume\":\"175 \",\"pages\":\"Article 108537\"},\"PeriodicalIF\":4.3000,\"publicationDate\":\"2024-10-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Intermetallics\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S096697952400356X\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, PHYSICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Intermetallics","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S096697952400356X","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, PHYSICAL","Score":null,"Total":0}
引用次数: 0
摘要
本研究探讨了粉末直接锻造对铝铁合金 Fe-28 的成分、结构和机械性能的影响。在合成和锻造 Fe3Al 粉末的过程中,在 1100 °C 的温度下形成了均匀的 A2 相。锻造后的孔隙率为 2-2.5%。残留孔隙主要呈平面状,位于粉末颗粒的边界。1300 °C退火可改善颗粒间边界的质量,所有样品都表现出跨晶断裂机制。在 1100 °C 下锻造并在 1300 °C 下退火的样品显示出最大强度 σbend = 1050 MPa 和断裂韧性 K1c = 32.3 MPa-m1/2。屈服强度显示出异常的温度敏感性,在 400 °C 和 500 °C 时达到最大值。在 600 °C 下测试的样品屈服强度有所下降,但足够高的屈服点 σy ∼400 MPa 和高强化率对高温抗蠕变性非常重要。在 600 °C、载荷为 120 兆帕的蠕变实验中,应变速率的变化范围为 10-7-10-6 s-1,速率灵敏度 n ≈ 4。蠕变的主要机制是位错滑行。
Mechanical behavior of powdered iron aluminide Fe – 28Al manufactured by direct powder forging
This study examines the impact of direct powder forging of powders on the composition, structure, and mechanical properties of iron aluminide Fe–28 at. % Al. During the synthesis and forging of Fe3Al powders, a homogeneous A2 phase is formed at a temperature of 1100 °C. Porosity after forging is 2–2.5 %. Residual pores are predominantly planar in shape and are located at the boundaries of the powder particles. Annealing at 1300 °C improves the quality of interparticle boundaries and all samples exhibit transcrystalline fracture mechanism. Samples forged at 1100 °C and annealed at 1300 °C show maximum strength σbend = 1050 MPa and fracture toughness K1c = 32.3 MPa·m1/2. The yield strength demonstrates anomalous temperature sensitivity with a maximum of 400 °C and at 500 °C. Samples tested at 600 °C show a decrease in yield strength, but a high enough yield point σy ∼400 MPa and a high strengthening rate are very important for high-temperature creep resistance. In creep experiments at a load of 120 MPa at 600 °C, the strain rate varies in the range of 10−7–10−6 s−1, the value of the rate sensitivity n ≈ 4. The main mechanism of creep is dislocation glide.
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