Ernesto Aguilar-Palazuelos, Perla Rosa Fitch-Vargas, Carlos Iván Delgado-Nieblas, Agustín López-Diaz, Aliette Gastélum-Ávila, Marco Antonio Sánchez-Chilero, Víctor Limón-Valenzuela, Irma Leticia Camacho-Hernández, Xóchitl Ariadna Ruiz-Armenta, Abraham Calderón-Castro
{"title":"基于玉米淀粉和明胶的可食用薄膜:挤压和浇铸工艺的结合:特性与应用","authors":"Ernesto Aguilar-Palazuelos, Perla Rosa Fitch-Vargas, Carlos Iván Delgado-Nieblas, Agustín López-Diaz, Aliette Gastélum-Ávila, Marco Antonio Sánchez-Chilero, Víctor Limón-Valenzuela, Irma Leticia Camacho-Hernández, Xóchitl Ariadna Ruiz-Armenta, Abraham Calderón-Castro","doi":"10.1007/s11483-024-09891-1","DOIUrl":null,"url":null,"abstract":"<div><p>The development of edible films (EFs) using renewable resources such as gelatin and native corn starch has garnered significant interest due to their potential to enhance food preservation and safety. Combining extrusion with the casting method enhances mechanical and barrier properties by modifying starch and gelatin structures through heat, pressure, and shear. This study aimed to develop, characterize, and optimize the functional properties EFs produced from an extruded formulation of corn starch, gelatin, and glycerol using the casting method. Furthermore, it evaluated the impact of these optimized EFs as coatings on the quality characteristics of the “Kent” mango cultivar. The study factors were gelatin content (GC, 0–10%) and extrusion temperature (ET, 80–120°C). The EFs were characterized and optimized, determining the tensile strength (<i>σ</i>), elongation (<i>ε</i>), water vapor permeability (WVP), and Water Solubility (S), using the surface response methodology. Results showed GC significantly influenced mechanical and barrier properties (<i>P <</i> 0.05), with higher GC increasing σ, ε, WVP, and S. ET also affected mechanical properties (<i>P <</i> 0.05) but not barrier properties (<i>P ></i> 0.05). EFs exhibited <i>σ</i> of 3.14 MPa to 8.34 MPa, <i>ε</i> of 10.55–25.60%, WVP (5.59 × 10<sup>–12</sup> to 6.82 × 10<sup>–11</sup> g m Pa<sup>-1</sup> s<sup>-1</sup> m<sup>-2</sup>), and S from 66.29–80.50%. According to the optimization study, the EFs with the best mechanical and barrier properties were obtained using an ET of 80°C and GC of 2.93%. Applied as coatings on ‘Kent’ mango, these EFs significantly extended shelf life and preserved postharvest quality.</p></div>","PeriodicalId":564,"journal":{"name":"Food Biophysics","volume":"20 1","pages":""},"PeriodicalIF":2.8000,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Edible Films Based on Corn Starch and Gelatin Obtained by the Combination of Extrusion and Casting Process: Characterization and Applications\",\"authors\":\"Ernesto Aguilar-Palazuelos, Perla Rosa Fitch-Vargas, Carlos Iván Delgado-Nieblas, Agustín López-Diaz, Aliette Gastélum-Ávila, Marco Antonio Sánchez-Chilero, Víctor Limón-Valenzuela, Irma Leticia Camacho-Hernández, Xóchitl Ariadna Ruiz-Armenta, Abraham Calderón-Castro\",\"doi\":\"10.1007/s11483-024-09891-1\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>The development of edible films (EFs) using renewable resources such as gelatin and native corn starch has garnered significant interest due to their potential to enhance food preservation and safety. 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引用次数: 0
摘要
利用明胶和原生玉米淀粉等可再生资源开发的可食用薄膜(EFs)因其在提高食品保存和安全性方面的潜力而备受关注。将挤压与浇铸方法相结合,通过热、压和剪切力改变淀粉和明胶的结构,可增强其机械和阻隔性能。本研究旨在利用浇铸法开发、表征和优化由玉米淀粉、明胶和甘油的挤压配方制成的功能特性 EFs。此外,研究还评估了这些优化后的 EF 作为涂层对 "肯特 "芒果品种质量特性的影响。研究因素包括明胶含量(GC,0-10%)和挤压温度(ET,80-120°C)。采用表面响应法对 EF 进行了表征和优化,确定了拉伸强度(σ)、伸长率(ε)、水蒸气渗透性(WVP)和水溶性(S)。结果表明,GC 对机械性能和阻隔性能有明显影响(P < 0.05),GC 越高,σ、ε、WVP 和 S 越大;ET 也影响机械性能(P < 0.05),但不影响阻隔性能(P > 0.05)。EF 的 σ 为 3.14 MPa 至 8.34 MPa,ε 为 10.55-25.60%,WVP 为 5.59 × 10-12 至 6.82 × 10-11 g m Pa-1 s-1 m-2,S 为 66.29-80.50%。根据优化研究,使用 80°C 的蒸发温度和 2.93% 的 GC,可获得机械和阻隔性能最佳的 EF。作为 "肯特 "芒果的涂层,这些 EF 能显著延长保质期并保持采后品质。
Edible Films Based on Corn Starch and Gelatin Obtained by the Combination of Extrusion and Casting Process: Characterization and Applications
The development of edible films (EFs) using renewable resources such as gelatin and native corn starch has garnered significant interest due to their potential to enhance food preservation and safety. Combining extrusion with the casting method enhances mechanical and barrier properties by modifying starch and gelatin structures through heat, pressure, and shear. This study aimed to develop, characterize, and optimize the functional properties EFs produced from an extruded formulation of corn starch, gelatin, and glycerol using the casting method. Furthermore, it evaluated the impact of these optimized EFs as coatings on the quality characteristics of the “Kent” mango cultivar. The study factors were gelatin content (GC, 0–10%) and extrusion temperature (ET, 80–120°C). The EFs were characterized and optimized, determining the tensile strength (σ), elongation (ε), water vapor permeability (WVP), and Water Solubility (S), using the surface response methodology. Results showed GC significantly influenced mechanical and barrier properties (P < 0.05), with higher GC increasing σ, ε, WVP, and S. ET also affected mechanical properties (P < 0.05) but not barrier properties (P > 0.05). EFs exhibited σ of 3.14 MPa to 8.34 MPa, ε of 10.55–25.60%, WVP (5.59 × 10–12 to 6.82 × 10–11 g m Pa-1 s-1 m-2), and S from 66.29–80.50%. According to the optimization study, the EFs with the best mechanical and barrier properties were obtained using an ET of 80°C and GC of 2.93%. Applied as coatings on ‘Kent’ mango, these EFs significantly extended shelf life and preserved postharvest quality.
期刊介绍:
Biophysical studies of foods and agricultural products involve research at the interface of chemistry, biology, and engineering, as well as the new interdisciplinary areas of materials science and nanotechnology. Such studies include but are certainly not limited to research in the following areas: the structure of food molecules, biopolymers, and biomaterials on the molecular, microscopic, and mesoscopic scales; the molecular basis of structure generation and maintenance in specific foods, feeds, food processing operations, and agricultural products; the mechanisms of microbial growth, death and antimicrobial action; structure/function relationships in food and agricultural biopolymers; novel biophysical techniques (spectroscopic, microscopic, thermal, rheological, etc.) for structural and dynamical characterization of food and agricultural materials and products; the properties of amorphous biomaterials and their influence on chemical reaction rate, microbial growth, or sensory properties; and molecular mechanisms of taste and smell.
A hallmark of such research is a dependence on various methods of instrumental analysis that provide information on the molecular level, on various physical and chemical theories used to understand the interrelations among biological molecules, and an attempt to relate macroscopic chemical and physical properties and biological functions to the molecular structure and microscopic organization of the biological material.