通过在钛基板上引爆喷涂前驱体盐获得的磷灰石涂层的拉曼研究

IF 2.1 4区物理与天体物理 Q3 PHYSICS, CONDENSED MATTER

Solid State Communications Pub Date : 2024-10-01 DOI:10.1016/j.ssc.2024.115710

I.P. Vorona , V.P. Temchenko , V.B. Lozinskii , M. Ya Valakh , IuM. Nasieka , V.A. Dubok , V.O. Yukhymchuk , A.E. Belyaev

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引用次数: 0

摘要

本文介绍了通过在钛基底上引爆喷涂前驱体盐而获得的磷灰石涂层的拉曼研究结果。Ca(OH)2 和 (NH4)2HPO4 盐摩尔比为 5:3 的混合物被用作前驱体。对最强烈拉曼光谱带的详细分析显示，羟基磷灰石的形成以无定形相为主。沉积后在 640 °C 的氩气环境中进行 30 分钟的热退火，可使无定形羟基磷灰石转变为晶体。

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Raman study of apatite coating, obtained by detonation spraying of the precursor salts on the titanium substrates

The results of the Raman study of the apatite coatings, obtained by detonation spraying of the precursor salts on the titanium substrates are presented. The mixture of Ca(OH)₂ and (NH₄)₂HPO₄ salts at the molar ratio 5:3 was used as precursors. A detailed analysis of the most intense Raman band showed hydroxyapatite formation with a dominant contribution of the amorphous phase. The post-deposition thermal annealing at 640 °C for 30 min in the Ar atmosphere leads to the transformation of the amorphous hydroxylapatite into the crystalline one.

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来源期刊

Solid State Communications 物理-物理：凝聚态物理

CiteScore

3.40

自引率

4.80%

发文量

287

审稿时长

51 days

期刊介绍： Solid State Communications is an international medium for the publication of short communications and original research articles on significant developments in condensed matter science, giving scientists immediate access to important, recently completed work. The journal publishes original experimental and theoretical research on the physical and chemical properties of solids and other condensed systems and also on their preparation. The submission of manuscripts reporting research on the basic physics of materials science and devices, as well as of state-of-the-art microstructures and nanostructures, is encouraged. A coherent quantitative treatment emphasizing new physics is expected rather than a simple accumulation of experimental data. Consistent with these aims, the short communications should be kept concise and short, usually not longer than six printed pages. The number of figures and tables should also be kept to a minimum. Solid State Communications now also welcomes original research articles without length restrictions. The Fast-Track section of Solid State Communications is the venue for very rapid publication of short communications on significant developments in condensed matter science. The goal is to offer the broad condensed matter community quick and immediate access to publish recently completed papers in research areas that are rapidly evolving and in which there are developments with great potential impact.