{"title":"研究在低压电弧放电等离子体中获得的氧化铜纳米粒子的磁感应特性","authors":"A. V. Ushackov, L. Yu. Fedorov","doi":"10.1134/S106378422407048X","DOIUrl":null,"url":null,"abstract":"<p>CuO nanoparticles obtained in a low-pressure arc discharge plasma followed by annealing in an oxygen atmosphere at 500°C were studied by X-ray diffraction and transmission electron microscopy. The formation of irregularly shaped nanoparticles in the size range of 5–30 nm was found. The Rietveld refinement confirmed the formation of a monoclinic CuO phase with an average crystallite size of ~21 nm. The temperature dependences of the magnetization and permittivity of CuO nanoparticles have been studied. They show antiferromagnetic behavior with a Neel temperature of 230 K and frequency-dependent dispersion behavior in the temperature range of 100–200 K at an external magnetic field induction of 0–1.3 T. The dielectric relaxation mechanism is analyzed and found to follow the Arrhenius behavior. It is shown that hopping conductivity with a variable hop length more accurately describes charge transport in CuO nanoparticles. A magnetodielectric response of about 2.5 was observed at a frequency of 12 kHz at a temperature of 150 K in a magnetic field of 1.3 T.</p>","PeriodicalId":783,"journal":{"name":"Technical Physics","volume":"69 7","pages":"2163 - 2169"},"PeriodicalIF":1.1000,"publicationDate":"2024-09-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Investigation of the Magnetic-Impedance Properties of CuO Nanoparticles Obtained in a Low-Pressure Arc Discharge Plasma\",\"authors\":\"A. V. Ushackov, L. Yu. Fedorov\",\"doi\":\"10.1134/S106378422407048X\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>CuO nanoparticles obtained in a low-pressure arc discharge plasma followed by annealing in an oxygen atmosphere at 500°C were studied by X-ray diffraction and transmission electron microscopy. The formation of irregularly shaped nanoparticles in the size range of 5–30 nm was found. The Rietveld refinement confirmed the formation of a monoclinic CuO phase with an average crystallite size of ~21 nm. The temperature dependences of the magnetization and permittivity of CuO nanoparticles have been studied. They show antiferromagnetic behavior with a Neel temperature of 230 K and frequency-dependent dispersion behavior in the temperature range of 100–200 K at an external magnetic field induction of 0–1.3 T. The dielectric relaxation mechanism is analyzed and found to follow the Arrhenius behavior. It is shown that hopping conductivity with a variable hop length more accurately describes charge transport in CuO nanoparticles. A magnetodielectric response of about 2.5 was observed at a frequency of 12 kHz at a temperature of 150 K in a magnetic field of 1.3 T.</p>\",\"PeriodicalId\":783,\"journal\":{\"name\":\"Technical Physics\",\"volume\":\"69 7\",\"pages\":\"2163 - 2169\"},\"PeriodicalIF\":1.1000,\"publicationDate\":\"2024-09-27\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Technical Physics\",\"FirstCategoryId\":\"101\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S106378422407048X\",\"RegionNum\":4,\"RegionCategory\":\"物理与天体物理\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"PHYSICS, APPLIED\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Technical Physics","FirstCategoryId":"101","ListUrlMain":"https://link.springer.com/article/10.1134/S106378422407048X","RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"PHYSICS, APPLIED","Score":null,"Total":0}
Investigation of the Magnetic-Impedance Properties of CuO Nanoparticles Obtained in a Low-Pressure Arc Discharge Plasma
CuO nanoparticles obtained in a low-pressure arc discharge plasma followed by annealing in an oxygen atmosphere at 500°C were studied by X-ray diffraction and transmission electron microscopy. The formation of irregularly shaped nanoparticles in the size range of 5–30 nm was found. The Rietveld refinement confirmed the formation of a monoclinic CuO phase with an average crystallite size of ~21 nm. The temperature dependences of the magnetization and permittivity of CuO nanoparticles have been studied. They show antiferromagnetic behavior with a Neel temperature of 230 K and frequency-dependent dispersion behavior in the temperature range of 100–200 K at an external magnetic field induction of 0–1.3 T. The dielectric relaxation mechanism is analyzed and found to follow the Arrhenius behavior. It is shown that hopping conductivity with a variable hop length more accurately describes charge transport in CuO nanoparticles. A magnetodielectric response of about 2.5 was observed at a frequency of 12 kHz at a temperature of 150 K in a magnetic field of 1.3 T.
期刊介绍：
Technical Physics is a journal that contains practical information on all aspects of applied physics, especially instrumentation and measurement techniques. Particular emphasis is put on plasma physics and related fields such as studies of charged particles in electromagnetic fields, synchrotron radiation, electron and ion beams, gas lasers and discharges. Other journal topics are the properties of condensed matter, including semiconductors, superconductors, gases, liquids, and different materials.
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