Yu. V. Bogatov, A. V. Shcherbakov, V. A. Shcherbakov, D. Yu. Kovalev, A. E. Sychev
{"title":"压力辅助电热爆炸合成镍化钛","authors":"Yu. V. Bogatov, A. V. Shcherbakov, V. A. Shcherbakov, D. Yu. Kovalev, A. E. Sychev","doi":"10.1134/S0020168523100011","DOIUrl":null,"url":null,"abstract":"<p>Titanium nickelide alloys have been prepared by pressure-assisted electrothermal explosion (ETE) synthesis. We have examined the effect of Joule heating power on ETE parameters and the physicomechanical properties of the synthesized alloys. The results demonstrate that raising the electrical voltage applied to the starting mixture leads to a decrease in ignition time and increase in the maximum ETE temperature. The ignition temperature was 350°C, independent of the Joule heating power. X-ray diffraction characterization showed that the major phase in the alloys was NiTi. According to uniaxial compression test results, the compressive strength of the alloys is 1980 MPa. Their microhardness <i>HV</i> is 6.4 ± 0.8 GPa. Instrumental indentation has been used to determine their hardness under load (<i>HM</i> = 9.4 GPa) and characteristics of their plastic and elastic deformation. The synthesized alloys have been shown to have high plasticity.</p>","PeriodicalId":585,"journal":{"name":"Inorganic Materials","volume":"59 10","pages":"1148 - 1154"},"PeriodicalIF":0.9000,"publicationDate":"2024-03-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Pressure-Assisted Electrothermal Explosion Synthesis of Titanium Nickelide\",\"authors\":\"Yu. V. Bogatov, A. V. Shcherbakov, V. A. Shcherbakov, D. Yu. Kovalev, A. E. Sychev\",\"doi\":\"10.1134/S0020168523100011\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Titanium nickelide alloys have been prepared by pressure-assisted electrothermal explosion (ETE) synthesis. We have examined the effect of Joule heating power on ETE parameters and the physicomechanical properties of the synthesized alloys. The results demonstrate that raising the electrical voltage applied to the starting mixture leads to a decrease in ignition time and increase in the maximum ETE temperature. The ignition temperature was 350°C, independent of the Joule heating power. X-ray diffraction characterization showed that the major phase in the alloys was NiTi. According to uniaxial compression test results, the compressive strength of the alloys is 1980 MPa. Their microhardness <i>HV</i> is 6.4 ± 0.8 GPa. Instrumental indentation has been used to determine their hardness under load (<i>HM</i> = 9.4 GPa) and characteristics of their plastic and elastic deformation. The synthesized alloys have been shown to have high plasticity.</p>\",\"PeriodicalId\":585,\"journal\":{\"name\":\"Inorganic Materials\",\"volume\":\"59 10\",\"pages\":\"1148 - 1154\"},\"PeriodicalIF\":0.9000,\"publicationDate\":\"2024-03-10\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Inorganic Materials\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S0020168523100011\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Inorganic Materials","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1134/S0020168523100011","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Pressure-Assisted Electrothermal Explosion Synthesis of Titanium Nickelide
Titanium nickelide alloys have been prepared by pressure-assisted electrothermal explosion (ETE) synthesis. We have examined the effect of Joule heating power on ETE parameters and the physicomechanical properties of the synthesized alloys. The results demonstrate that raising the electrical voltage applied to the starting mixture leads to a decrease in ignition time and increase in the maximum ETE temperature. The ignition temperature was 350°C, independent of the Joule heating power. X-ray diffraction characterization showed that the major phase in the alloys was NiTi. According to uniaxial compression test results, the compressive strength of the alloys is 1980 MPa. Their microhardness HV is 6.4 ± 0.8 GPa. Instrumental indentation has been used to determine their hardness under load (HM = 9.4 GPa) and characteristics of their plastic and elastic deformation. The synthesized alloys have been shown to have high plasticity.
期刊介绍:
Inorganic Materials is a journal that publishes reviews and original articles devoted to chemistry, physics, and applications of various inorganic materials including high-purity substances and materials. The journal discusses phase equilibria, including P–T–X diagrams, and the fundamentals of inorganic materials science, which determines preparatory conditions for compounds of various compositions with specified deviations from stoichiometry. Inorganic Materials is a multidisciplinary journal covering all classes of inorganic materials. The journal welcomes manuscripts from all countries in the English or Russian language.