{"title":"通过浸涂工艺在金属注射成型 316 不锈钢上真空烧结钛的微结构演变和性能","authors":"Cheng Liang , Bo-Cheng Shen , Shih-Hsien Chang , Muhtadin Muhtadin , Jung-Ting Tsai","doi":"10.1016/j.jmapro.2024.09.082","DOIUrl":null,"url":null,"abstract":"<div><div>Enhancing the surface coating of 316 L stainless steel, fabricated via metal injection molding, is crucial for its application in cost-effective, mass-produced components. This study investigated the titanium coating on 316 L stainless steel to address its limitations in mechanical performance. Titanium was coated on the 316 L stainless steel via a dip coating process, followed by vacuum sintering at temperatures of 1100 °C, 1150 °C, and 1200 °C. The optimal mechanical properties were achieved with a 100 μm thick coating sintered at 1200 °C, which exhibited uniformity and good bonding strength. The microstructure results demonstrated an average yield strength of 342.63 MPa and a polarization impedance of 968.48 Ω·cm<sup>2</sup>. Electron probe microanalysis confirmed the uniform diffusion of titanium into the stainless steel substrate, forming intermetallic phases such as Fe<sub>2</sub>Ti and NiTi. In addition, this study conducted a heat treatment process for the as-coated specimens. It was found that annealing at 750 °C for 4 h oil quenched and a 550 °C three-hour aging treatment the polarization impedance increases to 1243.3 Ω·cm<sup>2</sup> without compromising the yield strength. These findings indicate that the titanizing process enhances the mechanical properties of 316 L stainless steel, making it more suitable for demanding applications.</div></div>","PeriodicalId":16148,"journal":{"name":"Journal of Manufacturing Processes","volume":"131 ","pages":"Pages 1073-1085"},"PeriodicalIF":6.1000,"publicationDate":"2024-09-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microstructures evolution and properties of titanium vacuum sintering on metal injection molding 316 stainless steel via dip coating process\",\"authors\":\"Cheng Liang , Bo-Cheng Shen , Shih-Hsien Chang , Muhtadin Muhtadin , Jung-Ting Tsai\",\"doi\":\"10.1016/j.jmapro.2024.09.082\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Enhancing the surface coating of 316 L stainless steel, fabricated via metal injection molding, is crucial for its application in cost-effective, mass-produced components. This study investigated the titanium coating on 316 L stainless steel to address its limitations in mechanical performance. Titanium was coated on the 316 L stainless steel via a dip coating process, followed by vacuum sintering at temperatures of 1100 °C, 1150 °C, and 1200 °C. The optimal mechanical properties were achieved with a 100 μm thick coating sintered at 1200 °C, which exhibited uniformity and good bonding strength. The microstructure results demonstrated an average yield strength of 342.63 MPa and a polarization impedance of 968.48 Ω·cm<sup>2</sup>. Electron probe microanalysis confirmed the uniform diffusion of titanium into the stainless steel substrate, forming intermetallic phases such as Fe<sub>2</sub>Ti and NiTi. In addition, this study conducted a heat treatment process for the as-coated specimens. It was found that annealing at 750 °C for 4 h oil quenched and a 550 °C three-hour aging treatment the polarization impedance increases to 1243.3 Ω·cm<sup>2</sup> without compromising the yield strength. These findings indicate that the titanizing process enhances the mechanical properties of 316 L stainless steel, making it more suitable for demanding applications.</div></div>\",\"PeriodicalId\":16148,\"journal\":{\"name\":\"Journal of Manufacturing Processes\",\"volume\":\"131 \",\"pages\":\"Pages 1073-1085\"},\"PeriodicalIF\":6.1000,\"publicationDate\":\"2024-09-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Manufacturing Processes\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1526612524010028\",\"RegionNum\":1,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"ENGINEERING, MANUFACTURING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Manufacturing Processes","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1526612524010028","RegionNum":1,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MANUFACTURING","Score":null,"Total":0}
引用次数: 0
摘要
通过金属注射成型制造的 316 L 不锈钢要想应用于成本效益高的批量生产部件,增强其表面涂层至关重要。本研究对 316 L 不锈钢的钛涂层进行了研究,以解决其在机械性能方面的局限性。通过浸涂工艺在 316 L 不锈钢上镀钛,然后在 1100 ℃、1150 ℃ 和 1200 ℃ 的温度下进行真空烧结。在 1200 ℃ 下烧结的 100 μm 厚涂层具有均匀性和良好的结合强度,从而实现了最佳机械性能。微观结构结果表明,平均屈服强度为 342.63 兆帕,极化阻抗为 968.48 Ω-cm2。电子探针显微分析证实,钛均匀地扩散到不锈钢基体中,形成了金属间相,如 Fe2Ti 和 NiTi。此外,本研究还对涂层试样进行了热处理。结果发现,在 750 °C 下退火 4 小时后进行油淬,然后在 550 °C 下进行 3 小时的老化处理,极化阻抗会增加到 1243.3 Ω-cm2,而屈服强度不会受到影响。这些研究结果表明,钛化工艺提高了 316 L 不锈钢的机械性能,使其更适用于要求苛刻的应用领域。
Microstructures evolution and properties of titanium vacuum sintering on metal injection molding 316 stainless steel via dip coating process
Enhancing the surface coating of 316 L stainless steel, fabricated via metal injection molding, is crucial for its application in cost-effective, mass-produced components. This study investigated the titanium coating on 316 L stainless steel to address its limitations in mechanical performance. Titanium was coated on the 316 L stainless steel via a dip coating process, followed by vacuum sintering at temperatures of 1100 °C, 1150 °C, and 1200 °C. The optimal mechanical properties were achieved with a 100 μm thick coating sintered at 1200 °C, which exhibited uniformity and good bonding strength. The microstructure results demonstrated an average yield strength of 342.63 MPa and a polarization impedance of 968.48 Ω·cm2. Electron probe microanalysis confirmed the uniform diffusion of titanium into the stainless steel substrate, forming intermetallic phases such as Fe2Ti and NiTi. In addition, this study conducted a heat treatment process for the as-coated specimens. It was found that annealing at 750 °C for 4 h oil quenched and a 550 °C three-hour aging treatment the polarization impedance increases to 1243.3 Ω·cm2 without compromising the yield strength. These findings indicate that the titanizing process enhances the mechanical properties of 316 L stainless steel, making it more suitable for demanding applications.
期刊介绍:
The aim of the Journal of Manufacturing Processes (JMP) is to exchange current and future directions of manufacturing processes research, development and implementation, and to publish archival scholarly literature with a view to advancing state-of-the-art manufacturing processes and encouraging innovation for developing new and efficient processes. The journal will also publish from other research communities for rapid communication of innovative new concepts. Special-topic issues on emerging technologies and invited papers will also be published.