通过搅拌摩擦加工制备具有优异机械性能的细晶粒/超细晶粒 Nb521 合金

IF 6.2 2区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY
Haonan Wang , Bowen Li , Xin Xin , Wen Wang , Kuaishe Wang
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引用次数: 0

摘要

在铌合金中很难实现高强度和高延展性的协同作用。虽然通过剧烈塑性变形(SPD)技术实现了高强度,但却导致合金的低延展性。本研究采用 FSP 技术处理 Nb-5W-2Mo-1Zr-0.1C (Nb521)合金,制备出具有优异强度和延展性的细晶粒 (FG) / 超细晶粒 (UFG) Nb521。通过各种表征途径,系统研究了 Nb521 合金的微观结构演变和力学性能改善机理。研究结果表明,采用低肩切入深度快熔炉(LPD-FSP)可制备出晶粒尺寸为 0.63 ± 0.41 μm 的 UFG Nb521 合金,这是首次报道 UFG Nb521 合金。SZ 中形成洋葱圈结构的主要原因是搅拌工具的周期性磨损,洋葱圈结构不会造成机械损伤。Nb521 合金在不同加工参数下形成的纹理为离轴剪切纹理,与 D2(112-‾)[111] 旋转后的理想剪切纹理相吻合。此外,该研究还阐述了 Nb521 合金中第二相颗粒(Nb、Zr)C 在 FSP 过程中的细化机制。该研究还表明,室温下 FSP 样品屈服强度的提高主要是由晶粒细化决定的。这些发现为开发高性能铌合金提供了新思路。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Preparation of fine-grained/ultrafine-grained Nb521 alloy with superior mechanical property by friction stir processing

High strength-ductility synergy is difficult to achieve in Nb alloys. Although high strength has been achieved through severe plastic deformation (SPD) technology, led to low ductility in alloys. In this work, FSP technology was applied to treat Nb–5W–2Mo–1Zr-0.1C (Nb521) alloys in preparation of fine-grained (FG)/ultrafine-grained (UFG) Nb521 with excellent strength and ductility. The microstructure evolution and mechanical property improvement mechanism were systematically studied for Nb521 alloy through various characterization pathways. The research results indicated that UFG Nb521 alloy with a grain size of 0.63 ± 0.41 μm can be prepared using low shoulder plunge depth FSP (LPD-FSP), which is the first report of UFG Nb521 alloy. The main reason for the formation of onion rings structure in SZ is the periodic wear of the stirring tool, and the onion rings structure does not cause mechanical damage. The texture formed by Nb521 alloy under different processing parameters is off-axis shear texture, which matches the ideal shear texture of D2 (112)[111] after rotation. In addition, this study also elaborated on the refinement mechanism of the second phase particles (Nb, Zr) C in Nb521 alloy during FSP. This study also indicated that the increase in yield strength of FSP samples at room temperature is mainly determined by grain refinement. These findings provided new ideas for the development of high-performance niobium alloys.

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来源期刊
Journal of Materials Research and Technology-Jmr&t
Journal of Materials Research and Technology-Jmr&t Materials Science-Metals and Alloys
CiteScore
8.80
自引率
9.40%
发文量
1877
审稿时长
35 days
期刊介绍: The Journal of Materials Research and Technology is a publication of ABM - Brazilian Metallurgical, Materials and Mining Association - and publishes four issues per year also with a free version online (www.jmrt.com.br). The journal provides an international medium for the publication of theoretical and experimental studies related to Metallurgy, Materials and Minerals research and technology. Appropriate submissions to the Journal of Materials Research and Technology should include scientific and/or engineering factors which affect processes and products in the Metallurgy, Materials and Mining areas.
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