Rafael Magalhaes De Melo Freire, Shohei Uranaka, Eita Tochigi, Mitsuo Kimura, Tomoya Kawabata
{"title":"考虑到 4K 时预应变的影响,一种可变质奥氏体不锈钢及其氩弧焊焊接件在低温下因氢脆造成的延展性损失","authors":"Rafael Magalhaes De Melo Freire, Shohei Uranaka, Eita Tochigi, Mitsuo Kimura, Tomoya Kawabata","doi":"10.2355/isijinternational.isijint-2024-182","DOIUrl":null,"url":null,"abstract":"</p><p>The amount of martensite in austenitic stainless steels produced during plastic deformation at low temperatures is related to the reduction in hydrogen embrittlement resistance. A pre-strain at 4 K was employed in this work to produce strain-induced martensite (SIM) in the microstructure of SUS316L and its weldment to verify the changes in hydrogen embrittlement susceptibility through slow strain tensile (SSRT) tests in a high-pressure hydrogen environment. As the base metal specimens, the weld metal specimens, manufactured by gas tungsten arc welding (GTAW or TIG) were pre-strained at different levels (5%, 10%, and 15%) for comparison with the non-pre-strained condition. Analysis of the most degraded samples tested from -150 °C to 0 °C is conducted through fracture surface observations, lateral crack length measurement, and crack densities. It was possible to indicate that the pre-strain effect induced earlier crack nucleation in comparison to the situation observed in the non-pre-strained material. Moreover, the pre-existing martensite produced by the pre-strain at 4 K is responsible for earlier crack nucleation, leading to a loss in the hydrogen embrittlement resistance for the SSRT pre-strained base metal specimens.</p>\n<p></p>","PeriodicalId":14619,"journal":{"name":"Isij International","volume":"6 1","pages":""},"PeriodicalIF":1.6000,"publicationDate":"2024-09-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Ductility loss of a metastable austenitic stainless steel and its TIG weldment due to hydrogen embrittlement at low temperatures considering the effect of pre-strain at 4K\",\"authors\":\"Rafael Magalhaes De Melo Freire, Shohei Uranaka, Eita Tochigi, Mitsuo Kimura, Tomoya Kawabata\",\"doi\":\"10.2355/isijinternational.isijint-2024-182\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"</p><p>The amount of martensite in austenitic stainless steels produced during plastic deformation at low temperatures is related to the reduction in hydrogen embrittlement resistance. A pre-strain at 4 K was employed in this work to produce strain-induced martensite (SIM) in the microstructure of SUS316L and its weldment to verify the changes in hydrogen embrittlement susceptibility through slow strain tensile (SSRT) tests in a high-pressure hydrogen environment. As the base metal specimens, the weld metal specimens, manufactured by gas tungsten arc welding (GTAW or TIG) were pre-strained at different levels (5%, 10%, and 15%) for comparison with the non-pre-strained condition. Analysis of the most degraded samples tested from -150 °C to 0 °C is conducted through fracture surface observations, lateral crack length measurement, and crack densities. It was possible to indicate that the pre-strain effect induced earlier crack nucleation in comparison to the situation observed in the non-pre-strained material. Moreover, the pre-existing martensite produced by the pre-strain at 4 K is responsible for earlier crack nucleation, leading to a loss in the hydrogen embrittlement resistance for the SSRT pre-strained base metal specimens.</p>\\n<p></p>\",\"PeriodicalId\":14619,\"journal\":{\"name\":\"Isij International\",\"volume\":\"6 1\",\"pages\":\"\"},\"PeriodicalIF\":1.6000,\"publicationDate\":\"2024-09-18\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Isij International\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.2355/isijinternational.isijint-2024-182\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"METALLURGY & METALLURGICAL ENGINEERING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Isij International","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.2355/isijinternational.isijint-2024-182","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
引用次数: 0
摘要
奥氏体不锈钢在低温塑性变形过程中产生的马氏体数量与氢脆抗性的降低有关。本研究采用 4 K 预应变在 SUS316L 及其焊接件的微观结构中产生应变诱导马氏体 (SIM),通过高压氢环境下的慢应变拉伸 (SSRT) 试验验证氢脆敏感性的变化。作为母材试样,通过气体钨极氩弧焊(GTAW 或 TIG)制造的焊接金属试样在不同水平(5%、10% 和 15%)上进行了预应变,以便与非预应变状态进行比较。通过断裂面观察、横向裂纹长度测量和裂纹密度,对从 -150 °C 到 0 °C 测试的降解最严重的样品进行了分析。结果表明,与在非预拉伸材料中观察到的情况相比,预拉伸效应诱发了更早的裂纹成核。此外,在 4 K 温度下预应变产生的预存在马氏体是裂纹成核提前的原因,导致 SSRT 预应变基体金属试样的抗氢脆性能下降。
Ductility loss of a metastable austenitic stainless steel and its TIG weldment due to hydrogen embrittlement at low temperatures considering the effect of pre-strain at 4K
The amount of martensite in austenitic stainless steels produced during plastic deformation at low temperatures is related to the reduction in hydrogen embrittlement resistance. A pre-strain at 4 K was employed in this work to produce strain-induced martensite (SIM) in the microstructure of SUS316L and its weldment to verify the changes in hydrogen embrittlement susceptibility through slow strain tensile (SSRT) tests in a high-pressure hydrogen environment. As the base metal specimens, the weld metal specimens, manufactured by gas tungsten arc welding (GTAW or TIG) were pre-strained at different levels (5%, 10%, and 15%) for comparison with the non-pre-strained condition. Analysis of the most degraded samples tested from -150 °C to 0 °C is conducted through fracture surface observations, lateral crack length measurement, and crack densities. It was possible to indicate that the pre-strain effect induced earlier crack nucleation in comparison to the situation observed in the non-pre-strained material. Moreover, the pre-existing martensite produced by the pre-strain at 4 K is responsible for earlier crack nucleation, leading to a loss in the hydrogen embrittlement resistance for the SSRT pre-strained base metal specimens.
期刊介绍:
The journal provides an international medium for the publication of fundamental and technological aspects of the properties, structure, characterization and modeling, processing, fabrication, and environmental issues of iron and steel, along with related engineering materials.