{"title":"关于 Fe-3.2%Si 钢中取向晶粒异常生长的研究:热机械加工和抑制剂的作用","authors":"Pranabananda Modak , Kumar Aniket Anand , Abhijit Ghosh , Debalay Chakrabarti , Vinod Kumar","doi":"10.1016/j.matchemphys.2024.129850","DOIUrl":null,"url":null,"abstract":"<div><p>Detailed characterization of Fe-3.2%Si steel after different stages of processing trails including hot-rolling, normalization annealing, cold-rolling with intermediate annealing, and finally, decarburization/primary annealing and secondary annealing has been carried out. The evolution of ferrite grain structure, grain boundary characteristics, and the micro-texture of the samples are characterized using electron backscatter diffraction (EBSD). The inhibiting precipitates such as MnS and CuS are studied under scanning and transmission electron microscopy (SEM and TEM). The evolution of ferrite grain structure and texture are explained considering the mechanisms (role of inhibitors, crystal orientation, special boundary, high energy medium angle boundary, grain boundary curvature) responsible for the abnormal growth of Goss oriented grains after final annealing treatment. Extremely coarse Goss oriented grains (as large as >20 mm) have been developed in this study. An analytical approach is presented at the end to explain the texture evolution during processing considering the Taylor factor maps (for different loading conditions) and the prediction of limiting ferrite grain size for abnormal grain growth, considering the size and fraction of the precipitates along with their coarsening and dissolution kinetics.</p></div>","PeriodicalId":18227,"journal":{"name":"Materials Chemistry and Physics","volume":null,"pages":null},"PeriodicalIF":4.3000,"publicationDate":"2024-08-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Study on the abnormal growth of goss oriented grains in Fe-3.2%Si steel: Role of thermomechanical processing and inhibitors\",\"authors\":\"Pranabananda Modak , Kumar Aniket Anand , Abhijit Ghosh , Debalay Chakrabarti , Vinod Kumar\",\"doi\":\"10.1016/j.matchemphys.2024.129850\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Detailed characterization of Fe-3.2%Si steel after different stages of processing trails including hot-rolling, normalization annealing, cold-rolling with intermediate annealing, and finally, decarburization/primary annealing and secondary annealing has been carried out. The evolution of ferrite grain structure, grain boundary characteristics, and the micro-texture of the samples are characterized using electron backscatter diffraction (EBSD). The inhibiting precipitates such as MnS and CuS are studied under scanning and transmission electron microscopy (SEM and TEM). The evolution of ferrite grain structure and texture are explained considering the mechanisms (role of inhibitors, crystal orientation, special boundary, high energy medium angle boundary, grain boundary curvature) responsible for the abnormal growth of Goss oriented grains after final annealing treatment. Extremely coarse Goss oriented grains (as large as >20 mm) have been developed in this study. An analytical approach is presented at the end to explain the texture evolution during processing considering the Taylor factor maps (for different loading conditions) and the prediction of limiting ferrite grain size for abnormal grain growth, considering the size and fraction of the precipitates along with their coarsening and dissolution kinetics.</p></div>\",\"PeriodicalId\":18227,\"journal\":{\"name\":\"Materials Chemistry and Physics\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":4.3000,\"publicationDate\":\"2024-08-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Chemistry and Physics\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0254058424009787\",\"RegionNum\":3,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Chemistry and Physics","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0254058424009787","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Study on the abnormal growth of goss oriented grains in Fe-3.2%Si steel: Role of thermomechanical processing and inhibitors
Detailed characterization of Fe-3.2%Si steel after different stages of processing trails including hot-rolling, normalization annealing, cold-rolling with intermediate annealing, and finally, decarburization/primary annealing and secondary annealing has been carried out. The evolution of ferrite grain structure, grain boundary characteristics, and the micro-texture of the samples are characterized using electron backscatter diffraction (EBSD). The inhibiting precipitates such as MnS and CuS are studied under scanning and transmission electron microscopy (SEM and TEM). The evolution of ferrite grain structure and texture are explained considering the mechanisms (role of inhibitors, crystal orientation, special boundary, high energy medium angle boundary, grain boundary curvature) responsible for the abnormal growth of Goss oriented grains after final annealing treatment. Extremely coarse Goss oriented grains (as large as >20 mm) have been developed in this study. An analytical approach is presented at the end to explain the texture evolution during processing considering the Taylor factor maps (for different loading conditions) and the prediction of limiting ferrite grain size for abnormal grain growth, considering the size and fraction of the precipitates along with their coarsening and dissolution kinetics.
期刊介绍:
Materials Chemistry and Physics is devoted to short communications, full-length research papers and feature articles on interrelationships among structure, properties, processing and performance of materials. The Editors welcome manuscripts on thin films, surface and interface science, materials degradation and reliability, metallurgy, semiconductors and optoelectronic materials, fine ceramics, magnetics, superconductors, specialty polymers, nano-materials and composite materials.