三维打印钛合金的密度变化和生长方向对表面形貌以及与牙科树脂粘接性能的影响

Crystals Pub Date : 2024-08-08 DOI:10.3390/cryst14080712
Omar Alageel, N. Alfrisany, Abdullah Aldosari, Saud Qashish, Majed M. Alsarani, A. Alfaify
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引用次数: 0

摘要

钛基义齿是口腔修复学中必不可少的材料,现在可以通过控制工艺参数,使用粉末床融合(PBF)技术三维打印出不同密度的钛基义齿。本研究旨在评估由不同密度和生长方向的 3D 打印钛合金制成的牙科树脂的表面形貌和粘接强度。采用激光熔融三维打印技术制作了三组不同密度(低、中、高)的钛合金(Ti6Al4V)试样(N = 8)。每组包括垂直和水平生长的试样表面。测量了所有组钛样品的维氏硬度、表面粗糙度、润湿性和剪切结合强度(SBS)。还进行了扫描电子显微镜(SEM)检查。使用双向方差分析和费雪多重检验进行了统计分析。密度较高的试样显示出更高的显微硬度(p < 0.05),在同一密度类别中,水平生长方向的试样比垂直生长方向的试样更硬(p < 0.05)。此外,与其他组别相比,两个生长方向的低密度试样的表面粗糙度值最高(p < 0.05)。各组的润湿性值在垂直方向上相似(p > 0.05),但在水平方向上不相似(p < 0.05)。然而,密度类型对 3D 打印钛的粘接强度没有显著影响(p > 0.05)。本研究揭示了基于密度和生长方向的表面粗糙度、接触角和显微硬度的显著差异。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Impact of Density Variations and Growth Direction in 3D-Printed Titanium Alloys on Surface Topography and Bonding Performance with Dental Resins
Titanium-based dental prostheses are essential for prosthodontics and can now be 3D printed using powder bed fusion (PBF) technology with different densities by controlling the process parameters. This study aimed to assess the surface topography and bonding strength of dental resins made of 3D-printed titanium alloys with varying densities and growth directions. Three groups of titanium alloy (Ti6Al4V) specimens differentiated by density (low, medium, and high) were produced using laser-melting 3D printing technology (N = 8). Each group included specimen surfaces with vertical and horizontal growths. Vickers microhardness, surface profilometry, wettability, and shear bond strength (SBS) of the titanium samples were measured for all groups. Scanning electron microscopy (SEM) was performed. Statistical analyses were conducted using a two-way ANOVA and Fisher’s multiple test. Higher-density specimens exhibited greater microhardness (p < 0.05), and those with horizontal growth directions were harder (p < 0.05) than their vertical counterparts within the same density category. Additionally, low-density specimens in both growth directions had the highest surface roughness values (p < 0.05) compared to the other groups. The wettability values were similar (p > 0.05) among the groups in the vertical direction, but not in the horizontal direction (p < 0.05). However, the density type did not significantly (p > 0.05) influence the bonding strength of 3D-printed titanium. This study revealed significant variations in surface roughness, contact angle, and microhardness based on density and growth direction.
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