从高粱秸秆(Sorghum bicolor (L.) Moench)中合成纳米二氧化硅颗粒及其特性,并评估其对甜菜根(Beta vulgaris)种子萌发的影响

Patricia Ese Umoru, Abdullahi Maimuna, J. N. Akoji, Labaran Salihu
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摘要

研究人员采用溶胶-凝胶法合成了二氧化硅纳米粒子(Si-NPS),并对其进行了表征,同时还研究了其对蚕豆种子萌发的影响。Si-NPs 利用高粱秸秆合成,并使用傅立叶变换红外光谱仪 (FTIR)、X 射线衍射 (XRD)、扫描电子显微镜、扫描电子显微镜/能量色散光谱仪、X 射线光谱仪 (EDS) 进行表征。对合成的 Si-NPs 进行的结果评估显示如下:傅立叶变换红外光谱(FTIR)在 790.20、1051.10、1636.30 和 3403.10 cm-1 处显示出吸收带,分别表明存在 Si-H、Si-O-Si、Si-O 和 Si-OH。XRD 分析表明,Si-NPs 的平均粒径为 30.46 纳米。扫描电镜分析表明,Si-NPs 由无定形介孔结构组成。样品的元素组成为 65.33 % Si、12.77 % O、11.05 % Al、5.23 % Fe、3.42 % C 和 2.20 % Na。萌发研究结果表明,随着 Si-NPs 浓度(0-8 克/升)的增加,种子的萌发率和活力指数也随之增加,其中 8 克/升的种子萌发率最高。不含 Si-NPs 的对照组记录的秧苗生长量最少。对发芽时间的研究还表明,与对照组的发芽时间相比,Si-NPs 浓度最高(8 克/升)的种子发芽时间最短(2 天)。这项研究表明,Si-NPs 浓度的增加对甜菜根(Beta vulgaris)的发芽有积极影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and characterization of silica nanoparticles from sorghum straw (Sorghum bicolor (L.) Moench) and the evaluation of its effect on seed germination of Beta vulgaris (Beetroot)
The synthesis of silica nanoparticles (Si-NPS) using the sol-gel method and characterization, as well as their impact on the germination of Beta vulgaris seeds were investigated. Si-NPs were synthesized using sorghum straw, characterized using Fourier Transform Infrared Spectroscopy (FTIR), X-ray Diffraction (XRD), Scanning Electron Microscopy, SEM/Energy Dispersive Spectroscopy, X-ray Spectroscopy (EDS). Assessment of the results carried out on the synthesized Si-NPs revealed the following: FTIR showed absorption bands at 790.20, 1051.10, 1636.30, and 3403.10 cm-1 indicating the presence of Si-H, Si-O-Si, Si-O and Si-OH respectively. XRD analysis showed that the Si-NPs had an average size of 30.46 nm. SEM analysis showed that the Si-NPs were made up of amorphous mesoporous structures. The elemental composition of the sample was found to be 65.33 % Si, 12.77 % O, 11.05 % Al, 5.23 % Fe, 3.42 % C and 2.20 % Na. The result from the germination study demonstrated that as the concentration of Si-NPs increased from (0-8 g/L), the germination rate and vigour index of seeds also increased, with 8 g/L having the highest germinated seedlings. The control which has no Si-NPs recorded the least seedling growth. The study of the germination time also showed that seeds with the highest Si-NPs concentration of 8 g/L, germinated within the least germination period (2 days) when compared with the germination period of the control. This research has shown that increase in concentration of Si-NPs have a positive effect on the germination of Beta vulgaris (Beetroot).
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