Xizhi Sun, E. Heaps, A. Yacoot, Qingping Yang, Petr Grolich, P. Klapetek
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引用次数: 0
摘要
非光栅扫描可以提高原子力显微镜(AFM)的扫描帧频和测量速度。在非栅格扫描过程中还可以纠正三维漂移。不过,漂移校正算法取决于每个扫描模式的特性。虽然使用轮状扫描的局部非光栅扫描可能比常用的利萨如斯扫描模式更快,但漂移校正更具挑战性,因为扫描仅在局部相邻区段有交叉点,而交叉路径的时空间隔很短。本设计说明提出了一种新的解决方案,成功地克服了这一问题,并将以前为利萨如扫描开发的漂移校正方法扩展到使用玫瑰花扫描轨迹进行局部非光栅扫描的三维漂移校正。通过交叉点和对相同地物的局部重复扫描,可以确定 X、Y 和 Z 轴的漂移。在介绍一般程序的同时,还利用二维横向校准标准的轮状扫描进行了实验。实验结果表明,该方法能有效纠正三轴漂移和样本倾斜,从而显著改善图像质量。该方法只需要扫描中的局部交叉点,而不需要额外的扫描来确定基于交叉相关和最小二乘法技术的三维漂移,它可用于任何能够进行轮状扫描的原子力显微镜。
Three-dimensional drift correction of localised non-raster scanning on atomic force microscopy
Non-raster scanning can increase the scanning frame rate and measurement speed of atomic force microscopes (AFMs). It is also possible to correct the 3D drift during the non-raster scanning. However, the algorithm for the drift correction depends upon the properties of each scan pattern. While localised non-raster scanning using a rosette scan may be faster than the frequently used Lissajous scanning patterns, the drift correction is more challenging because the scan has crossing points only in local neighbouring segments where there are short temporal and spatial separations of the crossing paths. This design note presents a novel solution that successfully overcomes this problem and extends a drift correction method previously developed for Lissajous scans to the 3D drift correction of localised non-raster scanning using a rosette scan trajectory. The drift in the X, Y and Z axes can be determined using the crossing points and locally repeated scans of the same features. The general procedure is presented together with experiments using rosette scans of a two-dimensional lateral calibration standard. Experimental results have demonstrated that the method can effectively correct both the drift in the three axes and sample tilt, leading to significantly improved images. The method requires only localised crossing points in the scan and does not need additional scans to determine the three-dimensional drift based on cross-correlation and least squares techniques, and it can be used with any AFMs capable of rosette scanning.