Hui Tao, Hui-zhong Li, Li Wang, Rui Zhou, Yi-xuan Che, Yong-hui Chen, Xiao-peng Liang
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引用次数: 0
摘要
通过 X 射线衍射仪(XRD)、扫描电子显微镜(SEM)和透射电子显微镜(TEM)研究了锻造对高铌含量 Ti-45Al-7Nb-0.3W (at.%) 合金的微观结构和纹理演变的影响。结果表明,铸态合金主要由平均尺寸为 70 µm 的 α2/γ 片状菌落组成,但热锻薄饼显示出接近双相的微观结构(DP)。在热锻过程中,片状菌落会发生扭结和弯曲、变形孪晶和动态再结晶(DRX)。同时,锻造后β相中密集的位错表明,具有无序结构的高温β相有利于提高合金的热加工性能。与常见的 TiAl 铸造纹理不同,所研究的高 Nb 含量铸造合金的凝固过程完全通过 β 相区,从而形成了 <110>γ 纤维纹理,其中 <110>γ 平行于热流方向。相比之下,模锻合金中相对较强的<001>和较弱的<302>纹理成分归因于变形孪晶。退火后,孪晶边界和相交处会发生静态再结晶,从而削弱了变形纹理。
Effect of forging on the microstructure and texture of a high Nb containing γ-TiAl alloy
The effect of forging on the microstructure and texture evolution of a high Nb containing Ti-45Al-7Nb-0.3W (at.%) alloy was investigated by X-ray diffractometer (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The results show that the as-cast alloy is mainly composed of α2/γ lamellar colonies with a mean size of 70 µm, but the hot-forged pancake displays a near duplex microstructure (DP). Kinking and bending of lamellar colonies, deformation twinning and dynamic recrystallization (DRX) occur during hot forging. Meanwhile, dense dislocations in the β phase after forging suggest that the high-temperature β phase with a disordered structure is favorable for improving the hot-workability of the alloy. Unlike the common TiAl casting texture, the solidification process of the investigated as-cast alloy with high Nb content is completely via the β phase region, resulting in the formation of a <110>γ fiber texture where the <110>γ aligns parallel to the heat-flow direction. In comparison, the relatively strong <001> and weak <302> texture components in the as-forged alloy are attributed to the deformation twinning. After annealing, static recrystallization occurs at the twin boundary and intersections, which weakens the deformation texture.
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